Journal of Organometallic Chemistry p. 245 - 248 (1989)
Update date:2022-08-17
Topics:
Konishi, Hisatoshi
Matsumura, Chisato
Okano, Tamon
Kiji, Jitsuo
Treatment of 4-iodo-3H-phenothiazin-3-one with tetrakis(triphenylphosphine)palladium(0) in boiling benzene yields trans-iodo(3H-phenothiazin-3-one-4-yl)bis(triphenylphosphine)palladium(II) by oxidative addition. 5H-Benzo >phenothiazin-5-one-6-yl complex is prepared in a similar manner.The ?-bonded iminoquinone structure of the complexes has been elucidated by 1H, 13C, and 31P NMR spectroscopy.
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