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N,N-Bis(2-hydroxyethyl)ethylenediamine
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Name

N,N-Bis(2-hydroxyethyl)ethylenediamine

 EINECS 626-584-2
CAS No. 3197-06-6 Density 1.069
PSA 69.72000 LogP -1.06800
Solubility Soluble in water. Melting Point 92 °C
Formula C6H16N2O2 Boiling Point 291.7 °C at 760 mmHg
Molecular Weight 148.205 Flash Point 130.2 °C
Transport Information UN 2735 Appearance N/A
Safety 26-27-36/37/39-45 Risk Codes 34
Molecular Structure Molecular Structure of 3197-06-6 (N,N-Bis(2-hydroxyethyl)ethylenediamine) Hazard Symbols CorrosiveC
Synonyms

Ethanol,2,2'-[(2-aminoethyl)imino]di- (6CI,7CI,8CI);(2-Aminoethyl)bis(2-hydroxyethyl)amine;2,2'-[(2-Aminoethyl)imino]bisethanol;2-Amino-N,N-bis(2-hydroxyethyl)ethylamine;2-Bis[(2-hydroxyethyl)amino]ethylamine;N,N-Bis(2-hydroxyethyl)-1,2-diaminoethane;N,N-Bis(2-hydroxyethyl)ethanediamine;N,N-Bis(2-hydroxyethyl)ethylenediamine;N,N-Di(2-hydroxyethyl)ethylenediamine;N-(2-Aminoethyl)diethanolamine;NSC29614;[2-(Diethanolamino)ethyl]amine;

Article Data 10

N,N-Bis(2-hydroxyethyl)ethylenediamine Synthetic route

118839-29-5

N-(2phthalimidoethyl)diethanolamine

3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

Conditions
ConditionsYield
With hydrazine hydrate In methanol for 2.5h; Heating;80%
86241-19-2

2-(bis(2-hydroxyethyl)amino)acetonitrile

3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

Conditions
ConditionsYield
Stage #1: 2-(bis(2-hydroxyethyl)amino)acetonitrile With C46H178O41Si42; titanium(IV)isopropoxide In toluene at 60℃; for 24h; Inert atmosphere;
Stage #2: With water; sodium hydroxide In toluene at 20℃; for 4h; Inert atmosphere;		37%
With lithium aluminium tetrahydride In tetrahydrofuran Heating;
75-21-8

oxirane

1001-53-2

monoacetylaminoethylamine

3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

Conditions
ConditionsYield
With methanol und Erwaermen des Reaktionsprodukts mit wss.Salzsaeure;
(i) H2O, (ii) aq. NaOH; Multistep reaction;
(i) EtOH, (ii) aq. HCl; Multistep reaction;
107-15-3

ethylenediamine

111-42-2

2,2'-iminobis[ethanol]

3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

Conditions
ConditionsYield
With water at 100℃;
102-71-6

triethanolamine

A

110-85-0

piperazine

B

103-76-4

1-(2-hydroxyethyl)piperazine

C

140-31-8

aminoethylpiperazine

D

3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

Conditions
ConditionsYield
With ammonia; hydrogen; Ni/Re (6.8wtpercent/1.8wtpercent) on silica/alumina (80/20) at 170℃; under 85781.4 - 99537.9 Torr; for 10h; Product distribution / selectivity; Autoclave;
102-71-6

triethanolamine

A

103-76-4

1-(2-hydroxyethyl)piperazine

B

3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

Conditions
ConditionsYield
With ammonia; hydrogen; Ni/Re (6.8wtpercent/1.8wtpercent) on silica/alumina (80/20) at 165℃; under 85781.4 - 99537.9 Torr; for 4h; Product distribution / selectivity; Autoclave;
3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

1048697-12-6

4-N-octyl-N-methylaminosulfonyl-7-chloro-2,1,3-benzoxadiazole

1048697-05-7

4-(2'-N,N-diethanolaminoethyl)amino-7-N-octyl-N-methylaminosulfonyl-2,1,3-benzoxadiazole

Conditions
ConditionsYield
In acetonitrile at 60℃; for 4h;96%
3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

5147-80-8

[Bis(methylthio)methylene]malononitrile

111161-06-9

[1,3-bis(2-hydroxyethyl)imidazolidin-2-ylidene]malononitrile

Conditions
ConditionsYield
In tetrahydrofuran for 1h; Heating / reflux;95.3%
3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

224789-26-8

4-ethoxy-3-(5-methyl-4-oxo-7-propyl-3,4-dihydroimidazo[5,1-f][1,2,4]triazin-2-yl)-benzenelsulfonic acid chloride

N-2-{N,N-bis(2-hydroxyethyl)amino}ethyl-4-ethoxy-3-(5-methyl-4-oxo-7-propyl-3,4-dihydroimidazo[5,1-f][1,2,4]triazin-2-yl)benzenesulfonamide

Conditions
ConditionsYield
91%
3197-06-6

N,N-bis(2-hydroxyethyl)ethylidenediamine

192119-42-9

7-chloro-N,N-dimethylbenzo[c][1,2,5]oxadiazole-4-sulfonamide

1048696-96-3

4-(2'-N,N-diethanolaminoethyl)amino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole

Conditions
ConditionsYield
In acetonitrile at 60℃; for 4h;91%

N,N-Bis(2-hydroxyethyl)ethylenediamine Specification

The cas register number of N,N-Bis(2-hydroxyethyl)ethylenediamine is 3197-06-6. It also can be called as 2,2'-((2-Aminoethyl)imino)bisethanol and the Systematic name about this chemical is Ethanol, 2,2'-((2-aminoethyl)imino)bis-.

Physical properties about N,N-Bis(2-hydroxyethyl)ethylenediamine are: (1)ACD/LogP: -1.63; (2)ACD/LogD (pH 5.5): -4.92 ; (3)ACD/LogD (pH 7.4): -3.54 ; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 1; (7)ACD/KOC (pH 7.4): 1; (8)#H bond acceptors: 4; (9)#H bond donors: 4; (10)#Freely Rotating Bonds: 9; (11)Polar Surface Area: 24.94Å2; (12)Index of Refraction: 1.513; (13)Molar Refractivity: 40.17 cm3; (14)Molar Volume: 133.5 cm3; (15)Surface Tension: 52.2 dyne/cm; (16)Density: 1.109 g/cm3; (17)Flash Point: 130.2 °C; (18)Enthalpy of Vaporization: 61.63 kJ/mol; (19)Boiling Point: 291.7 °C at 760 mmHg; (20)Vapour Pressure: 0.000206 mmHg at 25°C.

When you are using this chemical, please be cautious about it as the following:
It is causes burns. If it in case of contact with eyes, rinse immediately with plenty of water and seek medical advice. People must take off immediately all contaminated clothing and wear suitable protective clothing, gloves and eye/face protection. In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)

People can use the following data to convert to the molecule structure.
1.SMILES: OCCN(CCN)CCO
2.InChI: InChI=1/C6H16N2O2/c7-1-2-8(3-5-9)4-6-10/h9-10H,1-7H2 
3.InChIKey: CYOIAXUAIXVWMU-UHFFFAOYAM
4.Std. InChI: InChI=1S/C6H16N2O2/c7-1-2-8(3-5-9)4-6-10/h9-10H,1-7H2 .

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