2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

Base Information

Chemical Name:2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile
CAS No.:23073-04-3
Molecular Formula:C18H17 N O3
Molecular Weight:295.3325
Hs Code.:
Mol file:23073-04-3.mol

Synonyms:Hydratroponitrile,b-p-anisoyl-p-methoxy- (6CI);Propionitrile, 3-p-anisoyl-2-(p-methoxyphenyl)- (8CI); NSC 249795

Suppliers and Price of 2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of 2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

Chemical Property:

Vapor Pressure:3.2E-10mmHg at 25°C
Boiling Point:502.4°Cat760mmHg
Flash Point:217.9°C
Density:1.149g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

There total 5 articles about 2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: potassium cyanide

: 41564-67-4
(E)-1,3-bis(4-methoxyphenyl)-2-propene-1-one

: 23073-04-3
2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

Guidance literature:: With acetic acid; In ethanol; water; for 2h; Reflux;
DOI:10.1039/d1ra02279b

Reference yield:

: 41564-67-4
(E)-1,3-bis(4-methoxyphenyl)-2-propene-1-one

: 151-50-8
potassium cyanide

: 23073-04-3
2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

Guidance literature:: With acetic acid; In 2-ethoxy-ethanol; at 105 ℃; for 0.5h;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 23073-04-3
2,4-bis(4-methoxyphenyl)-4-oxobutanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 10percent aq. NaOH / ethanol / 1.5 h / Ambient temperature

2: AcOH / H₂O; 2-ethoxy-ethanol / 0.5 h / 105 °C

With sodium hydroxide; acetic acid; In 2-ethoxy-ethanol; ethanol; water;
DOI:10.1021/jm9606507