2-Nitroisophthalamide

Base Information

Chemical Name:2-Nitroisophthalamide
CAS No.:32114-73-1
Molecular Formula:C8H7N3O4
Molecular Weight:209.161
Hs Code.:
DSSTox Substance ID:DTXSID40556596
Wikidata:Q82438196
Mol file:32114-73-1.mol

Synonyms:2-nitroisophthalamide;32114-73-1;2-nitrobenzene-1,3-dicarboxamide;1,3-Benzenedicarboxamide, 2-nitro-;2-nitro-isophthalamide;3-Carbamoyl-2-nitrobenzamide;SCHEMBL5792626;DTXSID40556596;SGVRCXLEYPXYIS-UHFFFAOYSA-N;MFCD12024397;AKOS015833489;AS-61872;W10310;A821134

Suppliers and Price of 2-Nitroisophthalamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2-Nitroisophthalamide

Chemical Property:

XLogP3:-0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:209.04365571
Heavy Atom Count:15
Complexity:277

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)C(=O)N)[N+](=O)[O-])C(=O)N

Technology Process of 2-Nitroisophthalamide

There total 3 articles about 2-Nitroisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1336-21-6
ammonium hydroxide

: 79-37-8
oxalyl dichloride

: dimethylformamide-methanol-ethyl acetate

: 21161-11-5
2-nitroisophthalic acid

: 32114-73-1
2-nitrobenzene-1,3-dicarboxamide

Guidance literature:: In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water;

Reference yield:

: 57053-00-6
2-nitro-1,3-benzenedicarbonyl chloride

: 32114-73-1
2-nitrobenzene-1,3-dicarboxamide

Guidance literature:: With ammonium hydroxide;

Reference yield:

: 81-20-9
2,6-dimethylnitrobenzene

: 32114-73-1
2-nitrobenzene-1,3-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; potassium permanganate / water / 23 h / 90 °C

2.1: thionyl chloride / N,N-dimethyl-formamide / 16 h / Inert atmosphere; Reflux

2.2: 6 h / 0 - 20 °C

With potassium permanganate; thionyl chloride; sodium hydroxide; In water; N,N-dimethyl-formamide;