Silanamine, 1,1,1-triethoxy-N,N-diethyl-

Base Information

• Chemical Name: Silanamine, 1,1,1-triethoxy-N,N-diethyl-
• CAS No.: 35077-00-0
• Molecular Formula: C10H25NO3Si
• Molecular Weight: 235.399
• European Community (EC) Number: 700-051-5
• UNII: M57Y78G8ML
• DSSTox Substance ID: DTXSID3074577
• Nikkaji Number: J2.155.974A
• Wikidata: Q82002858
• Mol file: 35077-00-0.mol

Synonyms:Silanamine, 1,1,1-triethoxy-N,N-diethyl-;35077-00-0;1,1,1-triethoxy-N,N-diethylsilanamine;Diethylaminotriethoxysilane;EC 700-051-5;N-ethyl-N-triethoxysilylethanamine;SCHEMBL22283;M57Y78G8ML;DTXSID3074577;NS00077423

Chemical Property of Silanamine, 1,1,1-triethoxy-N,N-diethyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 235.16037019
• Heavy Atom Count: 15
• Complexity: 137

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)[Si](OCC)(OCC)OCC

Technology Process of Silanamine, 1,1,1-triethoxy-N,N-diethyl-

There total 6 articles about Silanamine, 1,1,1-triethoxy-N,N-diethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

chlorotriethoxysilane (4667-99-6) + diethylamine (109-89-7) → tetraethoxy orthosilicate (78-10-4) + N-(triethoxysilyl)diethylamine (35077-00-0)

Guidance literature:

With triethylamine; In n-heptane; at 20 ℃; Product distribution / selectivity;

Reference yield:

(E)-styryl(triethoxy)silane (65119-09-7) + diethylamine (109-89-7) → styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + N-(triethoxysilyl)diethylamine (35077-00-0)

Guidance literature:

With carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; at 120 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4dt03084b

Reference yield:

trans-1-(triethoxylsilyl)-1-hexene (62621-32-3) + diethylamine (109-89-7) → 1-hexene (592-41-6,25067-06-5) + N-(triethoxysilyl)diethylamine (35077-00-0)

Guidance literature:

With carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; at 120 ℃; for 56h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4dt03084b

upstream raw materials:

chlorotriethoxysilane

diethylamine

dichlorodiethoxysilane

tetraethoxy orthosilicate

Downstream raw materials:

chlorotriethoxysilane

Refernces

• 1、 -. "PROCESS FOR PRODUCTION OF TRIALKOXYHALOSILANES, PROCESS FOR PRODUCTION OF ALKOXY(DIALKYLAMINO)SILANES, CATALYSTS FOR (CO)POLYMERIZATION OF ALPHA-OLEFINS, CATALYST COMPONENTS THEREFOR, AND PROCESS ES FOR POLYMERIZATION OF ALPHA-OLEFINS WITH THE CATALYSTS". Page/Page column 13. . Retrieved 2010/11/08.