Technology Process of Octanoic acid, 2-methylene-
There total 9 articles about Octanoic acid, 2-methylene- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
n-octyne; acetic acid;
With
iron pentacarbonyl; potassium tert-butylate;
In
tetrahydrofuran; dichloromethane;
at 25 ℃;
for 10h;
Inert atmosphere;
With
copper(II) choride dihydrate;
In
tetrahydrofuran; dichloromethane; acetone;
stereoselective reaction;
Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.01.005
- Guidance literature:
-
With
carbon monoxide;
palladium on activated charcoal; triphenylphosphine; 1,4-di(diphenylphosphino)-butane;
In
1,2-dimethoxyethane;
at 100 ℃;
for 24h;
under 5168 Torr;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00069a045
- Guidance literature:
-
With
carbon monoxide;
palladium on activated charcoal; triphenylphosphine; 1,4-di(diphenylphosphino)-butane;
In
1,2-dimethoxyethane;
at 100 ℃;
for 24h;
under 30400 Torr;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00069a045
