1-(4-methoxyphenyl)-N-[4-[(4-methoxyphenyl)methylideneamino]butyl]methanimine

Base Information

• Chemical Name: 1-(4-methoxyphenyl)-N-[4-[(4-methoxyphenyl)methylideneamino]butyl]methanimine
• CAS No.: 392686-87-2
• Molecular Formula: C20H24N2O2
• Molecular Weight: 324.423
• DSSTox Substance ID: DTXSID30405322

Synonyms:392686-87-2;ST51025884;DTXSID30405322;AKOS024380219

Chemical Property of 1-(4-methoxyphenyl)-N-[4-[(4-methoxyphenyl)methylideneamino]butyl]methanimine

Chemical Property:

• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 324.183778013
• Heavy Atom Count: 24
• Complexity: 332

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C=NCCCCN=CC2=CC=C(C=C2)OC

Technology Process of 1-(4-methoxyphenyl)-N-[4-[(4-methoxyphenyl)methylideneamino]butyl]methanimine

There total 2 articles about 1-(4-methoxyphenyl)-N-[4-[(4-methoxyphenyl)methylideneamino]butyl]methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-methoxy-benzaldehyde (123-11-5) + 1,4-diaminobutane (110-60-1) → N,N'-1,4-Tetramethylenebis[p-methoxybenzylidenealdimine] (392686-87-2)

Guidance literature:

In water; at 20 ℃; for 2h;

DOI:10.1039/b102749m

Reference yield:

1,4-diaminobutane (110-60-1) + 4-Methoxybenzyl alcohol (105-13-5) → N,N'-1,4-Tetramethylenebis[p-methoxybenzylidenealdimine] (392686-87-2)

Guidance literature:

With C₂₈H₂₈Cl₂Cu₂N₄; oxygen; potassium hydroxide; In toluene; at 60 ℃; for 8h;

DOI:10.1016/j.jorganchem.2017.05.009

Reference yield: 85.0%

N,N'-1,4-Tetramethylenebis[p-methoxybenzylidenealdimine] (392686-87-2) → N1,N4-bis(4-methoxybenzyl)butane-1,4-diamine (218956-13-9)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 2h;

DOI:10.1016/j.ejmech.2013.09.055

upstream raw materials:

4-methoxy-benzaldehyde

1,4-diaminobutane

4-Methoxybenzyl alcohol

Downstream raw materials:

C₂₄H₂₈N₂O₄S₂

3-[4-(4-Oxo-2-phenyl-thiazolidin-3-yl)-butyl]-2-phenyl-5-[1-phenyl-meth-(Z)-ylidene]-thiazolidin-4-one

N₁,N₄-bis(4-methoxybenzyl)butane-1,4-diamine

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