1α,2α-Bis[(trimethylsilyl)oxy]cyclohexane

Base Information

• Chemical Name: 1α,2α-Bis[(trimethylsilyl)oxy]cyclohexane
• CAS No.: 39789-20-3
• Molecular Formula: C12H28O2Si2
• Molecular Weight: 260.524
• Mol file: 39789-20-3.mol

Synonyms:cis-1,2-bis(trimethylsiloxy)cyclohexane;cis-1,2-bis-(trimethylsiloxy)cyclohexane;cis-1,2-Bis-trimethylsilyloxy-cyclohexan;cis-1,2-cyclohexanediyl bis(trimethylsilyl) ether;(1R,2S)-1,2-Bis-trimethylsilanyloxy-cyclohexane;

Chemical Property of 1α,2α-Bis[(trimethylsilyl)oxy]cyclohexane

Chemical Property:

• Boiling Point: 90 °C
• PSA: 18.46000
• LogP: 4.00060

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1α,2α-Bis[(trimethylsilyl)oxy]cyclohexane

There total 11 articles about 1α,2α-Bis[(trimethylsilyl)oxy]cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

chloro-trimethyl-silane (75-77-4) + 1,2-Cyclohexanediol (931-17-9) → cis-1,2-bis(trimethylsilyloxy)cyclohexane (39789-20-3)

Guidance literature:

With triethylamine; In dichloromethane; for 0.5h;

DOI:10.1016/j.tetlet.2014.12.044

Reference yield: 91.0%

cis-1,2-cyclohexane (1792-81-0) + 1,1,1,2,2,2-hexamethyldisilane (1450-14-2) → cis-1,2-bis(trimethylsilyloxy)cyclohexane (39789-20-3)

Guidance literature:

bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In N,N-dimethyl acetamide; at 80 ℃; for 3h;

DOI:10.1039/b608958e

Reference yield: 91.0%

1,1,1,2,2,2-hexamethyldisilane (1450-14-2) + (1R,2R)-trans-1,2-cyclohexanediol (1072-86-2,1460-57-7,1792-81-0,54383-22-1,57794-08-8,931-17-9) → trans-1,2-bis(trimethylsiloxy)cyclohexane (13871-93-7,39789-20-3,39789-21-4,125329-92-2)

Guidance literature:

bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In N,N-dimethyl acetamide; at 80 ℃; for 3h;

DOI:10.1039/b608958e

upstream raw materials:

chloro-trimethyl-silane

cis-1,2-cyclohexane

1,1,1,3,3,3-hexamethyl-disilazane

hexanedial

Downstream raw materials:

1,2-O-(2,3,4,6-tetra-O-benzyl-D-glucopyranosylidene)-cis-cyclohexandiol

C₁₈H₂₈O₅

(2S,3aS,7aR)-2-Benzyl-2-((R)-toluene-4-sulfinylmethyl)-hexahydro-benzo[1,3]dioxole

(2R,3aR,7aS)-2-Benzyl-2-((R)-toluene-4-sulfinylmethyl)-hexahydro-benzo[1,3]dioxole

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