Benzoic acid, 2,4,6-trimethyl-, 1-methylethyl ester

Base Information

• Chemical Name: Benzoic acid, 2,4,6-trimethyl-, 1-methylethyl ester
• CAS No.: 41589-61-1
• Molecular Formula: C13H18O2
• Molecular Weight: 206.28100
• Mol file: 41589-61-1.mol

Synonyms:Isopropyl-2,4,6-trimethylbenzoat;Mesitoesaeureisopropylester;2,4,6-Trimethylbenzoesaeure isopropylester;Isopropyl mesitylate;2,4,6-trimethyl-benzoic acid isopropyl ester;2,4,6-Trimethyl-benzoesaeure-isopropylester;

Chemical Property of Benzoic acid, 2,4,6-trimethyl-, 1-methylethyl ester

Chemical Property:

• PSA: 26.30000
• LogP: 3.17700

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2,4,6-trimethyl-, 1-methylethyl ester

There total 5 articles about Benzoic acid, 2,4,6-trimethyl-, 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-iodo-propane (75-30-9) + mesitylenecarboxylic acid (480-63-7) → isopropyl 2,4,6-trimethylbenzoate (41589-61-1)

Guidance literature:

With N(Et)4⁽¹⁺⁾*(2-pyrrolidone-anion); In N,N-dimethyl-formamide; for 1h; Ambient temperature;

DOI:10.1021/jo00354a030

Reference yield: 90.0%

mesitylenecarboxylic acid (480-63-7) + isopropyl alcohol (67-63-0,8013-70-5) → isopropyl 2,4,6-trimethylbenzoate (41589-61-1)

Guidance literature:

With pyridine; at 115 ℃; for 0.5h;

DOI:10.1246/bcsj.56.639

Reference yield: 85.0%

mesitylenecarboxylic acid (480-63-7) + isopropyl bromide (75-26-3) → isopropyl 2,4,6-trimethylbenzoate (41589-61-1)

Guidance literature:

With tetradecyl(trihexyl)phosphonium bistriflamide; N-ethyl-N,N-diisopropylamine; at 40 ℃;

DOI:10.1016/j.tetlet.2005.03.169

upstream raw materials:

mesitylenecarboxylic acid

isopropyl alcohol

2-iodo-propane

isopropyl bromide