3,4'-Bipyridine

Base Information

• Chemical Name: 3,4'-Bipyridine
• CAS No.: 4394-11-0
• Molecular Formula: C10H8N2
• Molecular Weight: 156.187
• DSSTox Substance ID: DTXSID10463263
• Nikkaji Number: J503.682H
• Wikidata: Q222998
• Mol file: 4394-11-0.mol

Synonyms:3,4'-Bipyridine;4394-11-0;SCHEMBL320526;DTXSID10463263;YTEIHWVCQJZNEN-UHFFFAOYSA-N;3-(PYRIDIN-4-YL)PYRIDINE;EN300-114808

Chemical Property of 3,4'-Bipyridine

Chemical Property:

• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 156.068748264
• Heavy Atom Count: 12
• Complexity: 130

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CN=C1)C2=CC=NC=C2

Technology Process of 3,4'-Bipyridine

There total 10 articles about 3,4'-Bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

C19H14N2O2 (30435-62-2) → 2,3'-bipyridine (581-50-0) + 3,4'-bipyridyl (4394-11-0) + 3,3'-bipyridine (581-46-4) + benzophenone (119-61-9)

Guidance literature:

In pyridine; Yield given. Further byproducts given; Ambient temperature; Irradiation;

DOI:10.1016/S0040-4039(01)91195-5

Reference yield: 44.0%

C19H14N2O2 (93845-12-6) → 4-(2-pyridyl)pyridine (581-47-5) + 4,4'-bipyridine (553-26-4) + 3,4'-bipyridyl (4394-11-0) + benzophenone (119-61-9)

Guidance literature:

In pyridine; Yield given. Further byproducts given; Ambient temperature; Irradiation;

DOI:10.1016/S0040-4039(01)91195-5

Reference yield: 25.0%

4-pyridyl phenyl sulfoxide (108770-97-4) → 4,4'-bipyridine (553-26-4) + 3,4'-bipyridyl (4394-11-0)

Guidance literature:

With pyridin-3-ylmagnesium bromide; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1016/S0040-4039(01)81070-4

upstream raw materials:

pyridine

C₁₉H₁₄N₂O₂

C₁₉H₁₄N₂O₂

pyridin-4-ylmagnesium bromide

Downstream raw materials:

3-(piperidin-4-yl)pyridine

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