1-(2-Phenylhydrazono)-1-(phenylazo)ethane

Base Information

• Chemical Name: 1-(2-Phenylhydrazono)-1-(phenylazo)ethane
• CAS No.: 4413-30-3
• Molecular Formula: C14H14N4
• Molecular Weight: 238.292
• Mol file: 4413-30-3.mol

Synonyms:C-Methyl-N,N'-diphenyl-formazan;Formazylmethane;3-Methyl-1.5-diphenyl-formazan;3-Methyl-1,5-diphenyl-formazan;1,5-diphenyl-3-methylformazan;N.N'-Diphenyl-C-methyl-formazan;

Chemical Property of 1-(2-Phenylhydrazono)-1-(phenylazo)ethane

Chemical Property:

• PSA: 49.11000
• LogP: 4.28880

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-Phenylhydrazono)-1-(phenylazo)ethane

There total 13 articles about 1-(2-Phenylhydrazono)-1-(phenylazo)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trimethyl-s-triazine (823-94-9) + phenylhydrazine (100-63-0) → N,N'-diphenyl-C-methylformazan (4413-30-3)

Guidance literature:

at 190 ℃; beim Aufbewahren des Reaktionsprodukts an der Luft;

DOI:10.1021/ja01568a047

Reference yield:

aniline (62-53-3) + acetaldehyde phenylhydrazone (935-07-9,20488-38-4,27935-60-0) → N,N'-diphenyl-C-methylformazan (4413-30-3)

Guidance literature:

With pyridine; hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.) water 2.) 0 deg C;

DOI:10.1016/0040-4020(82)80252-4

Reference yield:

benzene diazonium chloride (100-34-5) + pyruvic acid phenylhydrazone (5330-70-1,50705-99-2,50706-00-8) → N,N'-diphenyl-C-methylformazan (4413-30-3)

Guidance literature:

With alkali;

upstream raw materials:

2,4,6-trimethyl-s-triazine

phenylhydrazine

methyl-propanedioic acid

benzene diazonium chloride

Downstream raw materials:

5-methyl-2,3-diphenyl-tetrazolium; chloride

2,3-diphenyl-5-methyltetrazolium bromide

3-methylbenzo[e][1,2,4]triazine

1,2,3-Benzotriazole