1-Oxaspiro[4.5]dec-3-en-2-one

Base Information

Chemical Name:1-Oxaspiro[4.5]dec-3-en-2-one
CAS No.:4435-19-2
Molecular Formula:C9H12O2
Molecular Weight:152.193
Hs Code.:
DSSTox Substance ID:DTXSID70349099
Nikkaji Number:J427.797J
Wikidata:Q82124153

Synonyms:1-oxaspiro[4.5]dec-3-en-2-one;4435-19-2;SCHEMBL6113465;5,5-Pentanofuran-2(5H)-one;DTXSID70349099;1-oxaspiro[4.5]dec-3-en-2-on

Suppliers and Price of 1-Oxaspiro[4.5]dec-3-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-Oxaspiro[4.5]dec-3-en-2-one

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:152.083729621
Heavy Atom Count:11
Complexity:200

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC2(CC1)C=CC(=O)O2

Technology Process of 1-Oxaspiro[4.5]dec-3-en-2-one

There total 5 articles about 1-Oxaspiro[4.5]dec-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 82660-72-8
2',6'-exo-spirodioxatricyclo<5.2.1.0^2,6>dec-8'-en-3'-one>

: 110-00-9
furan

: 4435-19-2
1-oxa-spiro[4.5]dec-3-en-2-one

Guidance literature:: In tetrahydrofuran; at 130 ℃; under 7 Torr;
DOI:10.1021/jo00141a028

Reference yield: 32.0%

: 922-67-8
propynoic acid methyl ester

: 108-93-0
cyclohexanol

: 85728-60-5
methyl 3-(1'-hydroxycyclohex-1'-yl)prop-2E-enoate

: 4435-19-2
1-oxa-spiro[4.5]dec-3-en-2-one

Guidance literature:: With benzophenone; In acetonitrile; for 1.38333h; Irradiation;
DOI:10.1016/j.tetlet.2008.11.067

Reference yield: 23.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 922-67-8
propynoic acid methyl ester

: 699-61-6
1-oxaspiro[4.5]decan-2-one

: C₁₀H₁₆O₃

: 1428226-80-5
C₁₅H₂₂O₃

: 4435-19-2
1-oxa-spiro[4.5]dec-3-en-2-one

: 112247-22-0
methyl 2-(1-hydroxycyclohexyl)acrylate

Guidance literature:: With samarium diiodide; tert-butyl alcohol; In tetrahydrofuran; at 20 ℃; for 3h; Temperature;
DOI:10.1016/j.tetlet.2013.01.120