2,2,3,3,3-Pentafluoro-propionic acid hydrazide

Base Information

• Chemical Name: 2,2,3,3,3-Pentafluoro-propionic acid hydrazide
• CAS No.: 680-14-8
• Molecular Formula: C3H3F5N2O
• Molecular Weight: 178.0607
• Mol file: 680-14-8.mol

Synonyms:Pentafluorpropionsaeurehydrazid;N-(perfluoropropionyl)hydrazine;

Chemical Property of 2,2,3,3,3-Pentafluoro-propionic acid hydrazide

Chemical Property:

• Vapor Pressure: 3.33mmHg at 25°C
• Boiling Point: 153.4°C at 760 mmHg
• Flash Point: 46.6°C
• PSA: 55.12000
• Density: 1.548g/cm³
• LogP: 1.26510

Purity/Quality:

99% ^*data from raw suppliers

2,2,3,3,3-PENTAFLUORO-PROPIONIC ACID HYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,3,3,3-Pentafluoro-propionic acid hydrazide

There total 5 articles about 2,2,3,3,3-Pentafluoro-propionic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

perfluoropropionic acid methyl ester (378-75-6) + hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0) → Pentafluorpropionsaeurehydrazid (680-14-8)

Guidance literature:

In methanol; at 20°C (4 h) with 95 % N2H4 (dissolving in methanol);

DOI:10.1021/jo01069a054

Reference yield: 85.0%

2,2,3,3,3-pentafluoropropionamide (354-76-7) + hydrazine hydrate (7803-57-8,79785-97-0) → Pentafluorpropionsaeurehydrazid (680-14-8)

Guidance literature:

In diethyl ether; stirring by refluxing (2 h);

DOI:10.1021/jo01069a054

Reference yield: 73.0%

2-[1-Ethoxy-1-hydroxy-meth-(Z)-ylidene]-4,4,5,5,5-pentafluoro-3-oxo-pentanoic acid ethyl ester → Pentafluorpropionsaeurehydrazid (680-14-8)

Guidance literature:

With hydrazine; In diethyl ether; for 3.5h; -40 deg C to 20 deg C, other solvent aq. EtOH;

DOI:10.1007/BF00960661

upstream raw materials:

perfluoropropionic acid methyl ester

hydrazine

2,2,3,3,3-pentafluoropropionamide

hydrazine hydrate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 680-14-8 2,2,3,3,3-Pentafluoro-propionic acid hydrazide

Send

Send

Metric Ton KG G Pound L ML

Send

Send