3-Ethoxy-1,1'-biphenyl

Base Information

• Chemical Name: 3-Ethoxy-1,1'-biphenyl
• CAS No.: 54852-73-2
• Molecular Formula: C14H14O
• Molecular Weight: 198.265
• Hs Code.: 2909309090
• Mol file: 54852-73-2.mol

Synonyms:1,1‘-Biphenyl, 3-ethoxy-;3-ethoxybiphenyl;3-Aethoxy-biphenyl;3-Ethoxy-1,1'-biphenyl;Aethyl-biphenyl-3-yl-aether;1,1'-Biphenyl,3-ethoxy;ethyl-biphenyl-3-yl ether;3-Phenyl-phenetol;

Chemical Property of 3-Ethoxy-1,1'-biphenyl

Chemical Property:

• Vapor Pressure: 0.00152mmHg at 25°C
• Melting Point: 35°C
• Refractive Index: 1.5948 (estimate)
• Boiling Point: 305°Cat760mmHg
• Flash Point: 120.7°C
• PSA: 9.23000
• Density: 1.015g/cm³
• LogP: 3.75230

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Ethoxy-1,1'-biphenyl

There total 8 articles about 3-Ethoxy-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

m-ethoxyphenyl bromide (2655-84-7) + tributylphenylstannane (960-16-7) → 3-ethoxybiphenyl (54852-73-2)

Guidance literature:

With C₇₀H₄₀Cl₂F₆₈N₂O₆Pd₂; tetrabutylammomium bromide; In water; at 100 ℃; for 0.075h; Microwave irradiation;

DOI:10.1021/jo202482h

Reference yield: 82.0%

(3-ethoxyphenyl)boronic acid (90555-66-1) + chlorobenzene (108-90-7) → 3-ethoxybiphenyl (54852-73-2)

Guidance literature:

With C₇₀H₄₀Cl₂F₆₈N₂O₆Pd₂; tetrabutylammomium bromide; potassium carbonate; In water; at 140 ℃; for 0.2h; Microwave irradiation;

DOI:10.1021/jo202482h

Reference yield:

diethyl sulfate (64-67-5) + [1,1'-biphenyl]-3-ol (580-51-8) → 3-ethoxybiphenyl (54852-73-2)

Guidance literature:

With alkaline solution;

DOI:10.1021/ja01270a049

upstream raw materials:

diethyl sulfate

[1,1'-biphenyl]-3-ol

3-ethoxy-benzidine

ethyl iodide

Downstream raw materials:

biphenyl

cyclohexylcyclohexane

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