tetrahydroxyphosphonium dihydrogen phosphate - zinc (1:3) dihydrate

Base Information

• Chemical Name: tetrahydroxyphosphonium dihydrogen phosphate - zinc (1:3) dihydrate
• CAS No.: 7237-61-8
• Molecular Formula: H10O10P2Zn3
• Molecular Weight: 272.451

Synonyms:

Chemical Property of tetrahydroxyphosphonium dihydrogen phosphate - zinc (1:3) dihydrate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tetrahydroxyphosphonium dihydrogen phosphate - zinc (1:3) dihydrate

There total 1 articles about tetrahydroxyphosphonium dihydrogen phosphate - zinc (1:3) dihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aluminum (III) chloride (7446-70-0,7784-13-6) + diethyl ether (60-29-7,927820-24-4) + tert-butylmagnesium chloride (677-22-5) → tri-t-butyl aluminum etherate (7237-61-8) + di-t-butyl aluminum hydride etherate

Guidance literature:

aluminum (III) chloride; diethyl ether; tert-butylmagnesium chloride; at 20 - 25 ℃; for 24.5h; Inert atmosphere; Schlenk technique;

at -20 ℃; for 96h; Inert atmosphere; Schlenk technique;

DOI:10.1002/aoc.5961

Reference yield: 80.0%

3-Methylpyridine (108-99-6) + (tBu)3Al*OEt2 (7237-61-8) + 2-sulfanyl-1,3-benzoxazole (2382-96-9,118090-08-7) → [tBu2Al(OC6H4NCS)(NC5H4CH3)]

Guidance literature:

In diethyl ether; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2014.10.029

Reference yield: 75.0%

(tBu)3Al*OEt2 (7237-61-8) + 2-[(p-tolylamino)methyl]-4-(2,4,4-trimethylpentan-2-yl)phenol → C30H48AlNO

Guidance literature:

In diethyl ether; at -76 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1002/aoc.3748

upstream raw materials:

aluminum (III) chloride

diethyl ether

tert-butylmagnesium chloride

Downstream raw materials:

tBuAl(1,1,2,2-tetraphenylethane-1,2-diolate)(THF)

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