3,5-dichloropicolinaMide

Base Information

• Chemical Name: 3,5-dichloropicolinaMide
• CAS No.: 5468-71-3
• Molecular Formula: C6H4Cl2N2O
• Molecular Weight: 191.017
• Hs Code.: 2933399090
• Mol file: 5468-71-3.mol

Synonyms:3,5-dichloropyridine-2-carboxamide;

Chemical Property of 3,5-dichloropicolinaMide

Chemical Property:

• Vapor Pressure: 0.00314mmHg at 25°C
• Boiling Point: 283.5°Cat760mmHg
• PKA: 14.15±0.50(Predicted)
• Flash Point: 125.3°C
• PSA: 55.98000
• Density: 1.524g/cm³
• LogP: 2.18760
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

3,5-Dichloropicolinamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-dichloropicolinaMide

There total 2 articles about 3,5-dichloropicolinaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3,5-dichloropyridine-2-carboxylate (5439-08-7) → 3,5-dichloropicolinamide (5468-71-3)

Guidance literature:

With ammonia;

Reference yield:

→ 3,5-dichloropicolinamide (5468-71-3)

Guidance literature:

With thionyl chloride; In N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere;

With ammonium hydroxide; In dichloromethane; at 0 ℃;

Reference yield:

3,5-dichloropicolinamide (5468-71-3) + bromine (7726-95-6) + furan-2,3,5(4H)-trione pyridine (1:1) → 3,5-dichloropyridin-2-amine (4214-74-8)

Guidance literature:

upstream raw materials:

methyl 3,5-dichloropyridine-2-carboxylate

Downstream raw materials:

3,5-dichloropyridin-2-amine

C₁₈H₂₅ClN₄O₃

C₂₄H₃₁N₅O₄