Methyl 3,5-dichloropicolinate

Base Information

• Chemical Name: Methyl 3,5-dichloropicolinate
• CAS No.: 5439-08-7
• Molecular Formula: C7H5 Cl2 N O2
• Molecular Weight: 206.028
• Hs Code.: 2933399090
• Mol file: 5439-08-7.mol

Synonyms:NSC15054

Chemical Property of Methyl 3,5-dichloropicolinate

Chemical Property:

• Vapor Pressure: 0.00631mmHg at 25°C
• Boiling Point: 271.8°Cat760mmHg
• Flash Point: 118.2°C
• PSA: 39.19000
• Density: 1.426g/cm³
• LogP: 2.17500
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl3,5-dichloropicolinate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 3,5-dichloropicolinate

There total 9 articles about Methyl 3,5-dichloropicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + methyl 3,5-dichloropicolinic acid chloride (70151-22-3) → methyl 3,5-dichloropyridine-2-carboxylate (5439-08-7)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 1h;

Reference yield: 93.4%

methanol (67-56-1) + 3,5-dichloropyridine-2-carboxylic acid (81719-53-1) → methyl 3,5-dichloropyridine-2-carboxylate (5439-08-7)

Guidance literature:

With sulfuric acid; at 65 ℃; for 6h;

Reference yield:

3,5-dichloropyridine-2-carboxylic acid (81719-53-1) + diazomethyl-trimethyl-silane (18107-18-1) → methyl 3,5-dichloropyridine-2-carboxylate (5439-08-7)

Guidance literature:

In methanol; toluene; at 20 ℃; for 1h;

upstream raw materials:

methanol

methyl 3,5-dichloropicolinic acid chloride

3,5-dichloropyridine-2-carboxylic acid

3,5-dichloro-4-hydroxy-pyridine-2-carboxylic acid

Downstream raw materials:

3,5-dichloropicolinamide

3-chloro-5-(3-trifluoromethyl-phenyl)-pyridine-2-carboxylic acid methyl ester

3,5-bis-(3-trifluoromethyl-phenyl)-pyridine-2-carboxylic acid methyl ester

5-chloro-3-(3-trifluoromethyl-phenyl)-pyridine-2-carboxylic acid methyl ester