2-Cyclopentene-1-methanol, 4-hydroxy-, cis-

Base Information

Chemical Name:2-Cyclopentene-1-methanol, 4-hydroxy-, cis-
CAS No.:53837-32-4
Molecular Formula:C6H10O2
Molecular Weight:114.144
Hs Code.:
Mol file:53837-32-4.mol

Synonyms:

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Chemical Property of 2-Cyclopentene-1-methanol, 4-hydroxy-, cis-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2-Cyclopentene-1-methanol, 4-hydroxy-, cis-

There total 3 articles about 2-Cyclopentene-1-methanol, 4-hydroxy-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58101-60-3
methyl cyclopent-3-ene-1-carboxylate

: 53837-32-4
cis-4-Hydroxy-2-cyclopenten-1-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / camphorsulfonic acid / pyridine; CH₂Cl₂ / 24 h / Ambient temperature

2: 30percent aq. H₂O₂ / tetrahydrofuran / 2 h / Ambient temperature

3: 91 percent / lithium aluminium hydride / diethyl ether / 4 h / Ambient temperature

4: 3.8 mg / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 1 h; 2.) r.t., 2 days

With lithium aluminium tetrahydride; camphor-10-sulfonic acid; dihydrogen peroxide; boron tribromide; In tetrahydrofuran; pyridine; diethyl ether; dichloromethane;
DOI:10.1021/ja00326a019

Reference yield:

: 25125-21-7
4-(hydroxymethyl)cyclopentene

: 53837-32-4
cis-4-Hydroxy-2-cyclopenten-1-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / m-Cl-C₆H₄COOOH / CH₂Cl₂ / 20 h / Ambient temperature

2: 1.) NaBH₄, PhSeSePh, 2.) 30percent H₂O₂ / 1.) C₂H₅OH, 30 min, reflux, 2.) 1 h, r.t., C₂H₅OH

With sodium tetrahydroborate; diphenyl diselenide; dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;