2-Hydroxybenzoyl azide

Base Information

Chemical Name:2-Hydroxybenzoyl azide
CAS No.:54539-61-6
Molecular Formula:C7H5N3O2
Molecular Weight:163.136
Hs Code.:
DSSTox Substance ID:DTXSID90565577
Nikkaji Number:J1.715.210F
Wikidata:Q82450752

Synonyms:2-Hydroxybenzoyl azide;Salicylsaureazid;54539-61-6;DTXSID90565577

Suppliers and Price of 2-Hydroxybenzoyl azide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Hydroxybenzoyl azide

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:163.038176411
Heavy Atom Count:12
Complexity:223

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)N=[N+]=[N-])O

Technology Process of 2-Hydroxybenzoyl azide

There total 8 articles about 2-Hydroxybenzoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1441-87-8
salicyloyl chloride

: 54539-61-6
2-hydroxybenzoyl azide

Guidance literature:: With sodium azide; at 20 ℃;

Reference yield:

: C₁₉H₁₅O₄P

: 54539-61-6
2-hydroxybenzoyl azide

Guidance literature:: With dmap; sodium azide; In N,N-dimethyl-formamide; toluene; Inert atmosphere;
DOI:10.1021/acs.joc.9b01697

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 54539-61-6
2-hydroxybenzoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate

2: nitric acid; water

With water; nitric acid; hydrazine hydrate;