4-Phenyl-4-piperidinecarboxylic acid methyl ester

Base Information

• Chemical Name: 4-Phenyl-4-piperidinecarboxylic acid methyl ester
• CAS No.: 54824-07-6
• Molecular Formula: C13H17NO2
• Molecular Weight: 219.283
• Hs Code.: 2933399090
• Mol file: 54824-07-6.mol

Synonyms:methyl 4-phenylpiperidin-4-carboxylate;methyl 4-phenylpiperidine-4-carboxylate;4-phenyl-4-piperidinecarboxylic acid methyl ester;4-methoxycarbonyl-4-phenylpiperidine;4-(methoxycarbonyl)-4-phenylpiperidine;4-carbomethoxy-4-phenyl-piperidine;

Chemical Property of 4-Phenyl-4-piperidinecarboxylic acid methyl ester

Chemical Property:

• PSA: 38.33000
• LogP: 1.80960

Purity/Quality:

METHYL 4-PHENYLPIPERIDINE-4-CARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Phenyl-4-piperidinecarboxylic acid methyl ester

There total 9 articles about 4-Phenyl-4-piperidinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methanol (67-56-1) + 4-phenyl-4-piperidinecarboxylic acid 4-methylbenzenesulfonate → methyl 4-phenylpiperidine-4-carboxylate (54824-07-6)

Guidance literature:

With sulfuric acid; for 8h; Heating;

Reference yield: 88.0%

C20H23NO2 (76854-15-4) → methyl 4-phenylpiperidine-4-carboxylate (54824-07-6)

Guidance literature:

With palladium 10% on activated carbon; Pearlman's catalist; hydrogen; In methanol; for 6h; under 3102.97 Torr;

DOI:10.1248/cpb.57.1421

Reference yield:

1-tert-butyloxycarbonyl-4-phenyl-piperidine-4-carboxylic acid methyl ester (167262-47-7) → methyl 4-phenylpiperidine-4-carboxylate (54824-07-6)

Guidance literature:

With hydrogenchloride; In ethyl acetate;

DOI:10.1016/S0960-894X(00)00307-3

upstream raw materials:

N-(p-tosyl)-4-phenyl-4-cyano-piperidine

methanol

1-tert-butyloxycarbonyl-4-phenyl-piperidine-4-carboxylic acid methyl ester

benzeneacetic acid methyl ester

Downstream raw materials:

1-benzyl-4-[4-methoxycarbonyl-4-phenylpiperidin-1-yl]piperidine

3-(4-methoxycarbonyl-4-phenylpiperidin-1-yl)-3-methylpropionitrile

1-(4-Cyano-4,4-diphenylbutyl)-4-phenyl-4-piperidinecarboxylic acid, methyl ester

2-[4-methoxycarbonyl-4-phenylpiperidin-1-yl]ethylamine

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