N-(Dibenzofuran-2-yl)acetamide

Base Information

• Chemical Name: N-(Dibenzofuran-2-yl)acetamide
• CAS No.: 55232-39-8
• Molecular Formula: C14H11NO2
• Molecular Weight: 225.24300
• Mol file: 55232-39-8.mol

Synonyms:N-Dibenzofuran-2-yl-acetamide;N-Dibenzofuran-2-yl-acetamid;2-Acetamino-diphenylenoxid;2-Acetamino-dibenzofuran;N-(2-dibenzofuranyl)acetamide;

Chemical Property of N-(Dibenzofuran-2-yl)acetamide

Chemical Property:

• Melting Point: 166 - 167 °C
• PSA: 42.24000
• LogP: 3.61740

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(Dibenzofuran-2-yl)acetamide

There total 4 articles about N-(Dibenzofuran-2-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.9%

dibenzo[b,d]furan-2-amine (3693-22-9) + acetyl chloride (75-36-5) → N-dibenzofuran-2-yl-acetamide (55232-39-8)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.333333h;

Reference yield:

acetamide (60-35-5) + 2-bromodibenzo[b,d]furan (86-76-0) → N-dibenzofuran-2-yl-acetamide (55232-39-8)

Guidance literature:

With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In xylene; for 12h; Inert atmosphere; Reflux;

Reference yield:

dibenzo[b,d]furan-2-amine (3693-22-9) + acetic anhydride (108-24-7) → N-dibenzofuran-2-yl-acetamide (55232-39-8)

Guidance literature:

With benzene;

DOI:10.1021/ja01308a028

upstream raw materials:

dibenzo[b,d]furan-2-amine

acetic anhydride

acetamide

2-bromodibenzo[b,d]furan

Downstream raw materials:

N-(2-dibenzofuranyl)-N-phenylacetamide