Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]-

Base Information

• Chemical Name: Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]-
• CAS No.: 55339-64-5
• Molecular Formula: C10H22OSi
• Molecular Weight: 186.37
• DSSTox Substance ID: DTXSID90454992
• Nikkaji Number: J46.953J

Synonyms:2,4-Dimethyl-3-trimethylsiloxy-2-pentene;55339-64-5;Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]-;SCHEMBL4086971;DTXSID90454992;NTNHDIJDGWDRNM-UHFFFAOYSA-N;2,4-dimethyl-3-trimethylsilyloxy-2-pentene;2,4-dimethyl-3-trimethysilyloxy-2-pentene

Chemical Property of Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]-

Chemical Property:

• Boiling Point: 54 °C(Press: 11 Torr)
• PSA: 9.23000
• Density: 0.812±0.06 g/cm3(Predicted)
• LogP: 3.78780
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 186.143991855
• Heavy Atom Count: 12
• Complexity: 171

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(C)C(=C(C)C)O[Si](C)(C)C

Technology Process of Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]-

There total 1 articles about Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,O-bis-(trimethylsilyl)-acetamide (10416-59-8) + 2,4-dimethylpentan-3-one (565-80-0) → 2,4-dimethyl-3-trimethylsilyloxy-2-pentene (55339-64-5) + N-Trimethylsilylacetamide (13435-12-6)

Guidance literature:

With sodium; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 40 - 50 ℃;

DOI:10.1016/S0022-328X(00)85896-9

Reference yield: 96.0%

2,4-dimethyl-3-trimethylsilyloxy-2-pentene (55339-64-5) + (S)-2-phenyl-2-(phenylthio)ethanol (10277-56-2) → (5S)-2,4,4-trimethyl-5-phenyl-6-(phenylthio)-3-hexanone (140135-60-0)

Guidance literature:

With titanium tetrachloride; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1246/cl.1992.239

Reference yield: 93.0%

2,4-dimethyl-3-trimethylsilyloxy-2-pentene (55339-64-5) + (-)-carvyl acetate (97-42-7,1134-95-8,1205-42-1,5258-00-4,5258-01-5,7053-79-4,7111-29-7,76704-27-3,76704-28-4) → 2-(5-Isopropenyl-2-methyl-2-cyclohexen-1-yl)-2,4-dimethyl-3-pentanon (344438-52-4)

Guidance literature:

With zinc(II) iodide; In dichloromethane; Ambient temperature;

upstream raw materials:

N,O-bis-(trimethylsilyl)-acetamide

2,4-dimethylpentan-3-one

Downstream raw materials:

2,4,4,7-tetramethyl-oct-6-en-3-one

2,4-Dimethyl-2-(1,2,3,4-tetrahydro-1-naphthyl)-3-pentanon

2,4,4-trimethyl-5-phenyl-3-hexanone

2-Benzenesulfinyl-2,4-dimethyl-pentan-3-one

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