4H-1,3-Benzoxazin-4-one, 2-phenyl-, perchlorate

Base Information

• Chemical Name: 4H-1,3-Benzoxazin-4-one, 2-phenyl-, perchlorate
• CAS No.: 55424-93-6
• Molecular Formula: C14H9NO2.ClHO4
• Molecular Weight: 323.689
• DSSTox Substance ID: DTXSID90480099
• Mol file: 55424-93-6.mol

Synonyms:4H-1,3-Benzoxazin-4-one, 2-phenyl-, perchlorate;55424-93-6;DTXSID90480099

Chemical Property of 4H-1,3-Benzoxazin-4-one, 2-phenyl-, perchlorate

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 323.0196647
• Heavy Atom Count: 22
• Complexity: 445

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=NC(=O)C3=CC=CC=C3O2.OCl(=O)(=O)=O

Technology Process of 4H-1,3-Benzoxazin-4-one, 2-phenyl-, perchlorate

There total 1 articles about 4H-1,3-Benzoxazin-4-one, 2-phenyl-, perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzoylsalicylamide (5663-74-1) → 2-phenyl-4-oxo-1,3-benzoxazine perchlorate (55424-93-6)

Guidance literature:

With perchloric acid; In acetic anhydride; Heating;

Reference yield: 98.0%

2-phenyl-4-oxo-1,3-benzoxazine perchlorate (55424-93-6) → 5-(2-hydroxyphenyl)-3-phenyl-1,2,4-oxadiazole (79349-24-9)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In acetic acid; Heating;

DOI:10.1007/BF00767011

Reference yield: 98.0%

2-phenyl-4-oxo-1,3-benzoxazine perchlorate (55424-93-6) + phenylhydrazine (100-63-0) → 1,3-diphenyl-5-(o-hydroxyphenyl)-1,2,4-triazole (65483-97-8)

Guidance literature:

In acetic acid; Heating; oth. solvent;

upstream raw materials:

N-benzoylsalicylamide

Downstream raw materials:

2-(4-dimethylamino-phenyl)-2-phenyl-2,3-dihydro-benzo[e][1,3]oxazin-4-one

4-(allylthio)-2-(2-hydroxyphenyl)-6-phenyl-1,3,5-triazine

2-(4-Methylsulfanyl-6-phenyl-[1,3,5]triazin-2-yl)-phenol

5-(2-hydroxyphenyl)-3-phenyl-1,2,4-oxadiazole