Quinolin-8-yl 3-methyl-4-nitrobenzoate

Base Information

Chemical Name:Quinolin-8-yl 3-methyl-4-nitrobenzoate
CAS No.:5554-56-3
Molecular Formula:C₁₈H₁₉NO
Molecular Weight:265.355
Hs Code.:
DSSTox Substance ID:DTXSID10970881
Wikidata:Q82954175

Synonyms:quinolin-8-yl 3-methyl-4-nitrobenzoate;quinolin-8-yl 3-methyl-4-nitro-benzoate;Oprea1_537945;Oprea1_629028;DTXSID10970881;STK755477;AKOS000596020;AB00087060-01;Z28175887

Suppliers and Price of Quinolin-8-yl 3-methyl-4-nitrobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Quinolin-8-yl 3-methyl-4-nitrobenzoate

Chemical Property:

Vapor Pressure:6.17E-07mmHg at 25°C
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:308.07970687
Heavy Atom Count:23
Complexity:450

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)C(=O)OC2=CC=CC3=C2N=CC=C3)[N+](=O)[O-]

Technology Process of Quinolin-8-yl 3-methyl-4-nitrobenzoate

There total 8 articles about Quinolin-8-yl 3-methyl-4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 5554-55-2,54750-61-7
2,6-diphenyl-4-piperidone

: 74-88-4
methyl iodide

: 39653-65-1,5554-56-3
1-methyl-2,6-diphenyl-piperidin-4-one

Guidance literature:: With potassium carbonate; In acetone; at 45 - 55 ℃; for 3.5h;
DOI:10.1016/j.ejmech.2006.02.005

Reference yield: 73.0%

: 35225-79-7
dibenzylideneacetone

: 74-89-5
methylamine

: 39653-65-1,5554-56-3
1-methyl-2,6-diphenyl-piperidin-4-one

Guidance literature:: In ethanol; water; at 20 ℃; for 48h;

Reference yield:

: 100-52-7
benzaldehyde

: 39653-65-1,5554-56-3
1-methyl-2,6-diphenyl-piperidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaOH / H₂O; ethanol

2: 42 percent / dimethylformamide; H₂O

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide; 1: aldol reaction;
DOI:10.1016/j.bmc.2005.11.035