2-DIMETHYLAMINOMETHYL-BENZOIC ACID

Base Information

• Chemical Name: 2-DIMETHYLAMINOMETHYL-BENZOIC ACID
• CAS No.: 55741-01-0
• Molecular Formula: C10H13NO2
• Molecular Weight: 179.21600
• Mol file: 55741-01-0.mol

Synonyms:N,N-dimethylphthalamic acid;o-dimethylaminomethylbenzoic acid;o-N,N-dimethylaminomethylbenzoic acid;

Chemical Property of 2-DIMETHYLAMINOMETHYL-BENZOIC ACID

Chemical Property:

• Vapor Pressure: 0.003mmHg at 25°C
• Boiling Point: 274.819oC at 760 mmHg
• Flash Point: 120.007oC
• PSA: 40.54000
• Density: 1.13g/cm3
• LogP: 1.44640
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-[(dimethylamino)methyl]benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-DIMETHYLAMINOMETHYL-BENZOIC ACID

There total 3 articles about 2-DIMETHYLAMINOMETHYL-BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(bromomethyl)benzoic acid (7115-89-1) + dimethyl amine (124-40-3) → o-N,N-dimethylaminomethylbenzoic acid (55741-01-0)

Guidance literature:

In ethanol; water; at 20 ℃; for 12h;

DOI:10.1021/ja5016052

Reference yield:

2-((dimethylamino)methyl)benzonitrile (53369-76-9) → o-N,N-dimethylaminomethylbenzoic acid (55741-01-0)

Guidance literature:

With sulfuric acid; for 0.5h; Heating;

Reference yield:

→ o-N,N-dimethylaminomethylbenzoic acid (55741-01-0)

Guidance literature:

Komplex IXa, CO in Xylol;

DOI:10.1021/jo00906a021

upstream raw materials:

2-((dimethylamino)methyl)benzonitrile

2-(bromomethyl)benzoic acid

dimethyl amine

Downstream raw materials:

o-(N,N-dimethylaminomethyl)benzyl alcohol

((3R,4S,5S,7R,11R,12R,E)-12-ethyl-3,5,7,11-tetramethyl-2,8-dioxo-1-oxacyclododec-9-en-4-yl) 2-((dimethylamino)methyl)benzoate

C₂₇H₃₉NO₆

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