3-(6-Methoxynaphthalen-2-yl)butan-2-one

Base Information

Chemical Name:3-(6-Methoxynaphthalen-2-yl)butan-2-one
CAS No.:56600-77-2
Molecular Formula:C15H16O2
Molecular Weight:228.291
Hs Code.:
DSSTox Substance ID:DTXSID80535224

Synonyms:3-(6-Methoxynaphthalen-2-yl)butan-2-one;56600-77-2;SCHEMBL5534049;SCHEMBL20887114;DTXSID80535224;AKOS015781759

Suppliers and Price of 3-(6-Methoxynaphthalen-2-yl)butan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(6-Methoxynaphthalen-2-yl)butan-2-one

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:228.115029749
Heavy Atom Count:17
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=CC2=C(C=C1)C=C(C=C2)OC)C(=O)C

Technology Process of 3-(6-Methoxynaphthalen-2-yl)butan-2-one

There total 3 articles about 3-(6-Methoxynaphthalen-2-yl)butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5408-86-6
2,3-dibromobutane

: 5111-65-9
2-Bromo-6-methoxynaphthalene

: 93-04-9
2-Methoxynaphthalene

: 5111-66-0
6-Methoxy-2-naphthol

: 56600-77-2
3-(6-methoxy-2-naphthyl)-2-butanone

: 29619-45-2
6,6'-dimethoxy-2,2'-binaphthalene

: 2,2′-(1,2-dimethyl-1,2-ethanediyl)di-(6-methoxynaphthalene)

Guidance literature:: 2-Bromo-6-methoxynaphthalene; With magnesium; ethylene dibromide; In tetrahydrofuran; at 35 - 40 ℃; for 12.75h;

2,3-dibromobutane; With (FeCl₃)2(TMEDA)3; In tetrahydrofuran; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 598-32-3
2-hydroxy-3-butene

: 5111-65-9
2-Bromo-6-methoxynaphthalene

: 42924-53-8
nabumetone

: 56600-77-2
3-(6-methoxy-2-naphthyl)-2-butanone

Guidance literature:: 2-hydroxy-3-butene; With dicyclohexylmethylamine; tetrabutylammomium bromide; In N,N-dimethyl acetamide; at 20 ℃; for 0.25h;

2-Bromo-6-methoxynaphthalene; Kaiser oxime-derived complex on resin base; In N,N-dimethyl acetamide; at 120 ℃; for 14h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/adsc.200700301

Reference yield:

: 598-32-3
2-hydroxy-3-butene

: 5111-65-9
2-Bromo-6-methoxynaphthalene

: C₁₅H₁₆O₂

: 42924-53-8
nabumetone

: 56600-77-2
3-(6-methoxy-2-naphthyl)-2-butanone

Guidance literature:: 2-hydroxy-3-butene; With dicyclohexylmethylamine; tetrabutylammomium bromide; In N,N-dimethyl acetamide; at 20 ℃; for 0.25h;

2-Bromo-6-methoxynaphthalene; Kaiser oxime-derived complex on resin base; In N,N-dimethyl acetamide; at 120 ℃; for 24h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/adsc.200700301