N,N-DIETHYL-4-IODOBENZENAMINE

Base Information

• Chemical Name: N,N-DIETHYL-4-IODOBENZENAMINE
• CAS No.: 57702-49-5
• Molecular Formula: C10H14IN
• Molecular Weight: 275.132
• Mol file: 57702-49-5.mol

Synonyms:p-N,N-diethylaminoiodobenzene;4-Iodo-N,N-diethylaniline;N,N-diethyl-4-iodobenzenamine;Benzenamine,N,N-diethyl-4-iodo;

Chemical Property of N,N-DIETHYL-4-IODOBENZENAMINE

Chemical Property:

• PSA: 3.24000
• LogP: 3.13740

Purity/Quality:

99% ^*data from raw suppliers

N,N-DIETHYL-4-IODOBENZENAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-DIETHYL-4-IODOBENZENAMINE

There total 8 articles about N,N-DIETHYL-4-IODOBENZENAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N,N-diethylaniline (91-66-7) → N,N-diethyl-4-iodo-aniline (57702-49-5)

Guidance literature:

With bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate; In dichloromethane; for 0.166667h; Ambient temperature;

DOI:10.1016/0040-4039(95)01758-A

Reference yield: 88.0%

ethyl iodide (75-03-6) + p-aminoiodobenzene (540-37-4) → N,N-diethyl-4-iodo-aniline (57702-49-5)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 14h;

DOI:10.1002/ejoc.201200111

Reference yield: 74.0%

N,N-diethylaniline (93-05-0) → N,N-diethyl-4-iodo-aniline (57702-49-5)

Guidance literature:

N,N-diethylaniline; With water; sodium nitrite; In neat (no solvent); at 20 ℃;

With potassium iodide; In neat (no solvent); at 20 ℃;

DOI:10.1016/j.tetlet.2014.02.073

upstream raw materials:

N,N-diethylaniline

p-aminoiodobenzene

ethyl iodide

N,N-diethyl-O-benzoylhydroxylamine

Downstream raw materials:

dimethyl p-N,N-diethylaminobenzenephosphonate

1-(4-diethylaminophenyl)-4-n-hexyl-2,3-dioxopiperazine

3,5-dimethyl-2-(4-(N,N-diethylamino)phenyl)thiophene

N,N-diethyl-4-[(trimethylsilyl)ethynyl]aniline