1,2-Dichloro-1,1,2,2-tetramethyldistannane

Base Information

Chemical Name:1,2-Dichloro-1,1,2,2-tetramethyldistannane
CAS No.:58529-40-1
Molecular Formula:C4H12Cl2Sn2
Molecular Weight:368.465
Hs Code.:
DSSTox Substance ID:DTXSID00497774

Synonyms:58529-40-1;1,2-Dichloro-1,1,2,2-tetramethyldistannane;SCHEMBL11027103;DTXSID00497774

Suppliers and Price of 1,2-Dichloro-1,1,2,2-tetramethyldistannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1,2-Dichloro-1,1,2,2-tetramethyldistannane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:367.83541
Heavy Atom Count:8
Complexity:33

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Sn](C)Cl.C[Sn](C)Cl

Technology Process of 1,2-Dichloro-1,1,2,2-tetramethyldistannane

There total 10 articles about 1,2-Dichloro-1,1,2,2-tetramethyldistannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1,1,3-trimethyl-4-phenyl-1-stannacyclopent-3-ene

: 753-73-1
dimethyltin dichloride

: 85990-37-0
2-chloro-2,2,4,4-tetramethyl-1-oxa-3-chlora-2,4-distannacyclobutane dimer

: 18476-73-8
(3-methylbuta-1,3-dien-2-yl)benzene

: 58529-40-1
1,2-dichloro-tetramethyl-distannane

Guidance literature:: In Cyclohexane-d12; Reagent/catalyst; Photolysis;
DOI:10.1021/acs.organomet.5b00615

Reference yield:

: 1066-45-1
trimethyltin(IV)chloride

: 661-69-8
hexamethyldistannane

: 594-27-4
tetramethylstannane

: 753-73-1
dimethyltin dichloride

: 58529-40-1
1,2-dichloro-tetramethyl-distannane

Guidance literature:: With hydrogenchloride; In methanol; a mixt. of Me6Sn2 and Me3SnCl in MeOH was allowed to react for 70 h until a yellow colour characteristic of the "dimethyl polymer" appeared, one drop of 8.5 M aq. HCl was added, mixt. was kept for 10 min, reaction was followed by (1)H NMR spectroscopy; not isolated, identified by (1)H NMR spectrum;
DOI:10.1016/0022-328X(85)80064-4

Reference yield:

: 753-73-1
dimethyltin dichloride

: 16393-88-7
trimethyl(trimethylstannyl)silane

: 993-07-7
trimethylsilan

: 1066-45-1
trimethyltin(IV)chloride

: 594-27-4
tetramethylstannane

: 58529-40-1
1,2-dichloro-tetramethyl-distannane

: 16561-41-4
dimethyltin chloride

Guidance literature:: With methanol; In methanol; byproducts: Me3SiCl, Me3SiOSiMe3; a mixt. of Me3SiSnMe3 and Me2SiCl2 in methanol was kept for 150 min, reaction was followed by (1)H NMR spectroscopy; 70% of the substrate had been consumed, rate const. is given; not isolated, identified by (1)H NMR spectrum; Kinetics;
DOI:10.1016/0022-328X(85)80065-6