Alanine, N-[2-Methoxy-5-[[[(1E)-2-(2,4,6-triMethoxyphenyl)ethenyl]sulfonyl]Methyl]phenyl]-

Base Information

Chemical Name:Alanine, N-[2-Methoxy-5-[[[(1E)-2-(2,4,6-triMethoxyphenyl)ethenyl]sulfonyl]Methyl]phenyl]-
CAS No.:592542-82-0
Molecular Formula:C22H27NO8S
Molecular Weight:465.524
Hs Code.:
Mol file:592542-82-0.mol

Synonyms:racemic-(E)-2,4,6-trimethoxystyryl-3-(1-carboxyethyl)amino-4-methoxy-benzylsulfone;(E)-2,4,6-trimethoxystyryl-3-(1-carboxyethyl)amino-4-methoxybenzylsulfone;racemic-2-(5-(((E)-2,4,6-trimethoxystyrylsulfonyl)-methyl)-2-methoxyphenylamino)-propanoic acid;N-[2-METHOXY-5-[[[(1E)-2-(2,4,6-TRIMETHOXYPHENYL)ETHENYL]SULFONYL]METHYL]PHENYL]ALANINE;(E)-2-(5-((2,4,6-trimethoxystyrylsulfonyl)methyl)-2-methoxyphenylamino)propanoic acid;(E)-2-(5-(2,4,6-trimethoxystyrylsulfonylmethyl)-2-methoxyphenylamino)-propanoic acid;

Suppliers and Price of Alanine, N-[2-Methoxy-5-[[[(1E)-2-(2,4,6-triMethoxyphenyl)ethenyl]sulfonyl]Methyl]phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-[2-METHOXY-5-[[[(1E)-2-(2,4,6-TRIMETHOXYPHENYL)ETHENYL]SULFONYL]METHYL]PHENYL]ALANINE 95.00%
5MG
$ 499.85

Total 1 raw suppliers

Chemical Property of Alanine, N-[2-Methoxy-5-[[[(1E)-2-(2,4,6-triMethoxyphenyl)ethenyl]sulfonyl]Methyl]phenyl]-

Chemical Property:

PSA：128.77000
LogP:4.34550

Purity/Quality:: N-[2-METHOXY-5-[[[(1E)-2-(2,4,6-TRIMETHOXYPHENYL)ETHENYL]SULFONYL]METHYL]PHENYL]ALANINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Alanine, N-[2-Methoxy-5-[[[(1E)-2-(2,4,6-triMethoxyphenyl)ethenyl]sulfonyl]Methyl]phenyl]-

There total 15 articles about Alanine, N-[2-Methoxy-5-[[[(1E)-2-(2,4,6-triMethoxyphenyl)ethenyl]sulfonyl]Methyl]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 911294-96-7
(E)-methyl 2-(2-methoxy-5-((2',4',6'-trimethoxystyrylsulfonyl)methyl)phenylamino)propanoate

: 592542-82-0
(E)-2-(5-(2,4,6-trimethoxystyrylsulfonylmethyl)-2-methoxyphenylamino)-propanoic acid

Guidance literature:: With water; sodium hydroxide; In ethanol; Inert atmosphere;
DOI:10.1021/jm200570p

Reference yield:

: 119-10-8
4-methoxy-3-nitrotoluene

: 592542-82-0
(E)-2-(5-(2,4,6-trimethoxystyrylsulfonylmethyl)-2-methoxyphenylamino)-propanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 18 h / Inert atmosphere; Reflux

2.1: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere

3.1: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere

4.1: acetic acid; benzylamine / Inert atmosphere; Reflux

5.1: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere

6.1: sodium acetate / ethanol / 0.17 h / Inert atmosphere; Reflux

6.2: 48 h / Inert atmosphere; Reflux

7.1: water; sodium hydroxide / ethanol / Inert atmosphere

With N-Bromosuccinimide; sodium dithionite; water; dihydrogen peroxide; sodium acetate; acetic acid; benzylamine; sodium hydroxide; dibenzoyl peroxide; In methanol; tetrachloromethane; ethanol; water; acetone; 4.1: Knoevenagel condensation;
DOI:10.1021/jm200570p

Reference yield:

: 41870-24-0
(4-methoxy-3-nitrophenyl)methanol

: 592542-82-0
(E)-2-(5-(2,4,6-trimethoxystyrylsulfonylmethyl)-2-methoxyphenylamino)-propanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: phosphorus tribromide / toluene / 0.5 h / 40 - 100 °C / Inert atmosphere

2.1: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere

3.1: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere

4.1: acetic acid; benzylamine / Inert atmosphere; Reflux

5.1: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere

6.1: sodium acetate / ethanol / 0.17 h / Inert atmosphere; Reflux

6.2: 48 h / Inert atmosphere; Reflux

7.1: water; sodium hydroxide / ethanol / Inert atmosphere

With sodium dithionite; water; dihydrogen peroxide; sodium acetate; phosphorus tribromide; acetic acid; benzylamine; sodium hydroxide; In methanol; ethanol; water; acetone; toluene; 4.1: Knoevenagel condensation;
DOI:10.1021/jm200570p