trichloro(iodo)methane

Base Information

• Chemical Name: trichloro(iodo)methane
• CAS No.: 594-22-9
• Molecular Formula: CCl3I
• Molecular Weight: 245.274
• Mol file: 594-22-9.mol

Synonyms:

Chemical Property of trichloro(iodo)methane

Chemical Property:

• Vapor Pressure: 6.91mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trichloro(iodo)methane

There total 12 articles about trichloro(iodo)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrachloromethane (56-23-5) + iodine (7553-56-2,12190-71-5,8031-47-8) → 1,1,2,2-tetrachloroethylene (127-18-4) + trichloroiodomethane (594-22-9) + hexachloroethane (67-72-1) + Iodine monochloride (7790-99-0)

Guidance literature:

In tetrachloromethane; other Radiation; γ-radiation of I2 soln. in CCl4; yield depends on concn. of I2 and on dose of radiation;;

DOI:10.1021/j100671a004

Reference yield:

chloroform (67-66-3,8013-54-5) + iodine (7553-56-2,12190-71-5,8031-47-8) → trichloroiodomethane (594-22-9)

Guidance literature:

With sodium hydroxide; In neat (no solvent); formation on shaking CHCl3 with NaOH and iodine at room temp. for several days;;

DOI:10.1021/ja01941a008

Reference yield:

trichloroacetyl iodide (79929-41-2) → trichloroiodomethane (594-22-9)

Guidance literature:

In neat (no solvent); formation by destillation CCl3COI;;

DOI:10.1021/ja01871a061

upstream raw materials:

chloroform

Bromotrichloromethane

trichloroacetyl iodide

tetrachloromethane

Downstream raw materials:

dichlorocarbene

trichloromethyl radical

lithium iodide

tetrachloromethane