Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester

Base Information

• Chemical Name: Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester
• CAS No.: 630384-36-0
• Molecular Formula: C11H11IO2
• Molecular Weight: 302.112

Synonyms:4-iodophenylcyclopropyl acid methyl ester;CYCLOPROPANECARBOXYLIC ACID, 1-(4-IODOPHENYL)-, MEHTYL ESTER;

Chemical Property of Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester

Chemical Property:

• PSA: 26.30000
• LogP: 2.49580

Purity/Quality:

99%, ^*data from raw suppliers

CYCLOPROPANECARBOXYLICACID,1-(4-IODOPHENYL)-,MEHTYLESTER 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester

There total 3 articles about Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + 1-(4-iodophenyl)cyclopropane-1-carboxylic acid (124276-89-7) → 1-(4-iodophenyl)cyclopropanecarboxylic acid methyl ester (630384-36-0)

Guidance literature:

With chloro-trimethyl-silane; at 0 - 20 ℃;

Reference yield:

4-iodophenylacetonitrile (51628-12-7) → 1-(4-iodophenyl)cyclopropanecarboxylic acid methyl ester (630384-36-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / 60 °C

2.1: water; sodium hydroxide / 100 °C

2.2: pH 3 - 4

3.1: chloro-trimethyl-silane / 0 - 20 °C

With chloro-trimethyl-silane; N-benzyl-N,N,N-triethylammonium chloride; water; sodium hydroxide;

Reference yield:

1-(4-iodophenyl)cyclopropane-1-carbonitrile (124276-79-5) → 1-(4-iodophenyl)cyclopropanecarboxylic acid methyl ester (630384-36-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / 100 °C

1.2: pH 3 - 4

2.1: chloro-trimethyl-silane / 0 - 20 °C

With chloro-trimethyl-silane; water; sodium hydroxide;

upstream raw materials:

methanol

1-(4-iodophenyl)cyclopropane-1-carboxylic acid

4-iodophenylacetonitrile

1-(4-iodophenyl)cyclopropane-1-carbonitrile

Downstream raw materials:

4-(1-methoxycarbonyl-cyclopropyl)-benzoic acid

C₁₃H₁₂O₂

C₁₆H₂₀O₂Si

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