BIS-(2-VINYLOXY-ETHYL)-AMINE

Base Information

• Chemical Name: BIS-(2-VINYLOXY-ETHYL)-AMINE
• CAS No.: 13985-50-7
• Molecular Formula: C₈H₁₅NO₂
• Molecular Weight: 157.213
• Hs Code.: 2922199090
• Mol file: 13985-50-7.mol

Synonyms:Diethylamine,2,2'-bis(vinyloxy)- (6CI,7CI,8CI); Bis(2-allyloxyethyl)amine; Diethanolaminedivinyl ether; NSC 48510

Chemical Property of BIS-(2-VINYLOXY-ETHYL)-AMINE

Chemical Property:

• Vapor Pressure: 0.155mmHg at 25°C
• Boiling Point: 214.5°Cat760mmHg
• Flash Point: 83.6°C
• PSA: 30.49000
• Density: 0.912g/cm³
• LogP: 1.28710

Purity/Quality:

98%min ^*data from raw suppliers

Bis-(2-vinyloxy-ethyl)-amine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BIS-(2-VINYLOXY-ETHYL)-AMINE

There total 4 articles about BIS-(2-VINYLOXY-ETHYL)-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2'-iminobis[ethanol] (111-42-2) + acetylene (74-86-2,25067-58-7) → diethanolamine divinyl ether (13985-50-7)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 70 - 95 ℃; Product distribution; var. temp., var. time, other amount of KOH and DMSO;

Reference yield:

triethanolamine (102-71-6,64114-46-1) + acetylene (74-86-2,25067-58-7) → N-(2-vinyloxyethyl)morpholine (16486-81-0) + diethanolamine divinyl ether (13985-50-7) + N,N,N-tris[2-(vinyloxy)ethyl]amine (1559-68-8)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) DMSO, 70 deg C, 20 min, 2.) DMSO, 100 deg C, 10 h;

Reference yield:

triethanolamine (102-71-6,64114-46-1) + acetylene (74-86-2,25067-58-7) → N-(2-vinyloxyethyl)morpholine (16486-81-0) + diethanolamine divinyl ether (13985-50-7) + bis-(2-hydroxy-ethyl)-(2-vinyloxy-ethyl)-amine (1559-70-2) + 2-[bis-(2-vinyloxy-ethyl)-amino]-ethanol (1559-69-9)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) DMSO, 70 deg C, 20 min, 2.) DMSO, 115eg C, 4h;

upstream raw materials:

2,2'-iminobis[ethanol]

acetylene

triethanolamine

Downstream raw materials:

bis-(2-ethoxyethyl)amine

Bis-<2-vinyloxy-aethyl>-phenylmercaptomethyl-amin

potassium bis-N-(vinyloxyethyl)dithiocarbamate