BIS(2-ETHOXYETHYL)AMINE

Base Information

• Chemical Name: BIS(2-ETHOXYETHYL)AMINE
• CAS No.: 124-21-0
• Molecular Formula: C8H19 N O2
• Molecular Weight: 161.244
• Hs Code.: 2922199090
• Mol file: 124-21-0.mol

Synonyms:3,9-Dioxa-6-azaundecane(5CI); Diethylamine, 2,2'-diethoxy- (7CI,8CI); 2,2'-Diethoxydiethylamine;Bis(2-ethoxyethyl)amine; N,N-Bis(2-ethoxyethyl)amine

Chemical Property of BIS(2-ETHOXYETHYL)AMINE

Chemical Property:

• Melting Point: -50°C
• Refractive Index: 1.4200-1.4230
• Boiling Point: 200 °C
• PKA: 8.62±0.19(Predicted)
• Flash Point: 77.4oC
• PSA: 30.49000
• Density: 0.89
• LogP: 1.03990

Purity/Quality:

98% ^*data from raw suppliers

Bis(2-ethoxyethyl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BIS(2-ETHOXYETHYL)AMINE

There total 6 articles about BIS(2-ETHOXYETHYL)AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N-benzyl-2-ethoxy-N-(2-ethoxyethyl)ethanamine (288852-82-4) → bis-(2-ethoxyethyl)amine (124-21-0)

Guidance literature:

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; at 120 ℃; for 6h; under 5700.38 Torr;

DOI:10.1021/jo000175r

Reference yield:

N,N-bis-(2-ethoxy-ethyl)-aniline (139474-24-1) → bis-(2-ethoxyethyl)amine (124-21-0)

Guidance literature:

With hydrogenchloride; sodium nitrite; und Kochen des Reaktionsprodukts mit wss.NaHSO₃-Loesung;

Reference yield:

2-ethoxy-ethanol (110-80-5) → bis-(2-ethoxyethyl)amine (124-21-0)

Guidance literature:

With phosphoric acid; pumice stone; ammonia;

upstream raw materials:

2-ethoxy-ethanol

2-ethoxy-1-ethanamine

2-chloroethyl ethyl ether

diethanolamine divinyl ether

Downstream raw materials:

Bis-(2-ethoxy-ethyl)-(6-{N'-[1-phenyl-meth-(E)-ylidene]-hydrazino}-pyridazin-3-yl)-amine

Refernces

• 1、 Tanaka, Mutsuo,Kamada, Kenji,Ando, Hisanori,Kitagaki, Takashi,Shibutani, Yasuhiko,Kimura, Keiichi. "Synthesis and Photochromism of Crowned Spirobenzothiapyran: Facilitated Photoisomerization by Cooperative Complexation of Crown Ether and Thiophenolate Moieties with Metal Ions". . p. 4342 - 4347. Retrieved 2007/10/03.