3-methyl-4-[(E)-(4-nitrophenyl)diazenyl]aniline

Base Information

• Chemical Name: 3-methyl-4-[(E)-(4-nitrophenyl)diazenyl]aniline
• CAS No.: 62308-10-5
• Molecular Formula: C₁₃H₁₂N₄O₂
• Molecular Weight: 256.264
• Hs Code.: 2927000090
• Mol file: 62308-10-5.mol

Synonyms:3-methyl-4-(4-nitrophenyl)diazenyl-aniline;p-Nitrobenzol-azo-m-toluidin;3-methyl-4-(4-nitro-phenylazo)-aniline;(4-Nitro-benzol)-(1 azo 6)-(3-amino-toluol);3-METHYL-4-((4-NITROPHENYL)AZO)BENZENAMINE;4'-Nitro-4-amino-2-methyl-azobenzol;4'-Amino-2'-methyl-4-nitro-azobenzol;

Chemical Property of 3-methyl-4-[(E)-(4-nitrophenyl)diazenyl]aniline

Chemical Property:

• Vapor Pressure: 2.67E-09mmHg at 25°C
• Boiling Point: 478°Cat760mmHg
• Flash Point: 242.9°C
• PSA: 96.56000
• Density: 1.31g/cm³
• LogP: 5.00520

Purity/Quality:

4-AMINO-2-METHYL-4'-NITROAZOBENZENE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methyl-4-[(E)-(4-nitrophenyl)diazenyl]aniline

There total 3 articles about 3-methyl-4-[(E)-(4-nitrophenyl)diazenyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrobenzenediazonium chloride (100-05-0) + m-toluidine hydrochloride (638-03-9) → 3-methyl-4-(4-nitro-phenylazo)-aniline (62308-10-5)

Guidance literature:

With sodium acetate; man kocht das Rohprodukt mit Salzsaeure, wobei das nebenher gebildete 4'-Nitro-3-methyl-diazoaminobenzol zersetzt wird;

Reference yield:

4-nitrobenzenediazonium chloride (100-05-0) + 1-amino-3-methylbenzene (108-44-1) → 3-methyl-4-(4-nitro-phenylazo)-aniline (62308-10-5) + N-(4-nitro-phenyl)-N'-m-tolyl-triazene (132942-70-2)

Guidance literature:

With pyridine;

Reference yield:

4-nitrobenzenediazonium chloride (100-05-0) + sodium acetate (127-09-3) → 3-methyl-4-(4-nitro-phenylazo)-aniline (62308-10-5) + N-(4-nitro-phenyl)-N'-m-tolyl-triazene (132942-70-2)

Guidance literature:

upstream raw materials:

4-nitrobenzenediazonium chloride

m-toluidine hydrochloride

1-amino-3-methylbenzene

sodium acetate