Cyclobutanecarboxamide, N-methoxy-N-methyl- (9CI)

Base Information

• Chemical Name: Cyclobutanecarboxamide, N-methoxy-N-methyl- (9CI)
• CAS No.: 640768-72-5
• Molecular Formula: C7H13NO2
• Molecular Weight: 143.186
• Hs Code.: 2921490090
• Mol file: 640768-72-5.mol

Synonyms:N-Methoxy-N-methyl-cyclobutanecarboxamide;cyclobutanecarboxylic acid N-methoxy-N-methylamide;Cyclobutanecarboxamide,N-methoxy-N-methyl;N-methoxy-N-methylcyclobutylcarboxamide;cyclobutanecarboxylic acid methoxy-methyl-amide;

Chemical Property of Cyclobutanecarboxamide, N-methoxy-N-methyl- (9CI)

Chemical Property:

• Boiling Point: 176.8±23.0 °C(Predicted)
• PSA: 29.54000
• Density: 1.081±0.06 g/cm3(Predicted)
• LogP: 0.80630
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

N-methoxy-N-methylcyclobutanecarboxamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclobutanecarboxamide, N-methoxy-N-methyl- (9CI)

There total 5 articles about Cyclobutanecarboxamide, N-methoxy-N-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) + Cyclobutanecarbonyl chloride (5006-22-4) → cyclobutanecarboxylic acid N-methoxy-N-methylamide (640768-72-5)

Guidance literature:

N,O-dimethylhydroxylamine*hydrochloride; With triethylamine; In dichloromethane; at 0 ℃;

Cyclobutanecarbonyl chloride; In dichloromethane; at 4 - 23 ℃;

DOI:10.1021/acs.jmedchem.7b00008

Reference yield: 86.0%

N,0-dimethylhydroxylamine (1117-97-1) + Cyclobutanecarbonyl chloride (5006-22-4) → cyclobutanecarboxylic acid N-methoxy-N-methylamide (640768-72-5)

Guidance literature:

With pyridine; at 25 ℃; Inert atmosphere;

DOI:10.1021/ol101639g

Reference yield: 72.0%

methyl cyclobutanecarboxylate (765-85-5) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → cyclobutanecarboxylic acid N-methoxy-N-methylamide (640768-72-5)

Guidance literature:

methyl cyclobutanecarboxylate; N,O-dimethylhydroxylamine*hydrochloride; In tetrahydrofuran; at -20 ℃; for 0.0833333h; Inert atmosphere;

With isopropylmagnesium chloride; In tetrahydrofuran; diethyl ether; at -20 ℃; for 0.416667h; Inert atmosphere;

DOI:10.1039/c3ob40578h

upstream raw materials:

Cyclobutanecarboxylic acid

N,O-dimethylhydroxylamine*hydrochloride

N,0-dimethylhydroxylamine

Cyclobutanecarbonyl chloride

Downstream raw materials:

(5-chloro-2-thienyl)(cyclobutyl)methanone

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