Acetamide, N,N,2-triphenyl-

Base Information

• Chemical Name: Acetamide, N,N,2-triphenyl-
• CAS No.: 33675-70-6
• Molecular Formula: C20H17NO
• Molecular Weight: 287.361
• Hs Code.: 2924299090
• NSC Number: 97591
• DSSTox Substance ID: DTXSID30294657
• Nikkaji Number: J122.215E
• Wikidata: Q82034052
• ChEMBL ID: CHEMBL1902630
• Mol file: 33675-70-6.mol

Synonyms:Acetamide, N,N,2-triphenyl-;N,N,2-Triphenylacetamide;33675-70-6;2,N,N-Triphenylacetamide;Benzeneacetamide, N,N-diphenyl-;MLS002703411;ACETAMIDE,N,N,2-TRIPHENYL-;NSC97591;Acetamide,N,2-triphenyl-;Cambridge id 5247623;Benzeneacetamide,N-diphenyl-;N,N,2-Triphenylacetamide #;Oprea1_127296;SCHEMBL1792495;CHEMBL1902630;DTXSID30294657;OJJDDQBPSFGSOH-UHFFFAOYSA-N;NSC-97591;CCG-328738;SMR001570130

Chemical Property of Acetamide, N,N,2-triphenyl-

Chemical Property:

• Vapor Pressure: 1.15E-10mmHg at 25°C
• Boiling Point: 513.8°Cat760mmHg
• Flash Point: 249°C
• PSA: 20.31000
• Density: 1.157g/cm³
• LogP: 4.59400
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 287.131014166
• Heavy Atom Count: 22
• Complexity: 318

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CC(=O)N(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Acetamide, N,N,2-triphenyl-

There total 6 articles about Acetamide, N,N,2-triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

diphenylamine (122-39-4) + phenylacetyl chloride (103-80-0) → N-phenylacetyldiphenylamine (33675-70-6)

Guidance literature:

With triethylamine; In dichloromethane; Inert atmosphere;

DOI:10.1021/acs.organomet.8b00835

Reference yield: 79.0%

carbon monoxide (201230-82-2) + sodium 2-benzylidene-1-tosylhydrazin-1-ide (27992-27-4,40154-38-9) + diphenylamine (122-39-4) → N-phenylacetyldiphenylamine (33675-70-6)

Guidance literature:

With potassium phosphate; cobalt(II) 5,10,15,20-tetraphenylporphyrin; In toluene; at 50 ℃; for 18h; under 7500.75 Torr; Inert atmosphere; Autoclave;

DOI:10.1002/chem.201301731

Reference yield: 73.0%

carbon monoxide (201230-82-2) + N,N-diphenylbenzylamine (606-87-1) → N-phenylacetyldiphenylamine (33675-70-6)

Guidance literature:

N,N-diphenylbenzylamine; With ortho-diphenylphosphinobenzoic acid; nickel dichloride; for 0.5h; Glovebox; Autoclave;

carbon monoxide; With iodine; at 140 ℃; for 48h; under 15201 Torr; Glovebox; Autoclave;

DOI:10.1021/acs.orglett.7b01488

upstream raw materials:

diphenylamine

phenylacetyl chloride

N.N-Diphenyl-α-chlorphenylacetamid

carbon monoxide

Downstream raw materials:

acridine

carbon monoxide

Diphenylmethane

4-(diphenylmethyl)aniline