3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester

Base Information

Chemical Name:3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester
CAS No.:6493-78-3
Molecular Formula:C9H14O2
Molecular Weight:154.209
Hs Code.:
DSSTox Substance ID:DTXSID10447967
Nikkaji Number:J540.994B

Synonyms:6493-78-3;3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester;3-Methyl-3-cyclohexene-1-carboxylic acid methyl ester;DTXSID10447967;ALWNXIRSKYWVFP-UHFFFAOYSA-N;1-carbomethoxy-3-methylcyclohex-3-ene

Suppliers and Price of 3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:154.099379685
Heavy Atom Count:11
Complexity:182

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCCC(C1)C(=O)OC

Technology Process of 3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester

There total 9 articles about 3-Cyclohexene-1-carboxylic acid, 3-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 78-79-5,9003-31-0
isoprene

: 6493-79-4,5443-14-1
methyl 4-methyl-3-cyclohexene-1-carboxylate

: 6493-78-3,637000-43-2
3-methyl-3-cyclohexene-1-carboxylic acid methyl ester

Guidance literature:: With zeolite Beta; In dichloromethane; Heating;

Reference yield:

: 4-Benzenesulfonyl-3-methyl-cyclohex-3-enecarboxylic acid methyl ester

: 6493-78-3,637000-43-2
3-methyl-3-cyclohexene-1-carboxylic acid methyl ester

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In methanol; at 25 ℃; for 48h; Yield given;
DOI:10.1021/jo00201a034

Reference yield:

: 67-56-1
methanol

: 814-68-6,25189-84-8
acryloyl chloride

: 78-79-5,9003-31-0
isoprene

: 6493-78-3,637000-43-2
3-methyl-3-cyclohexene-1-carboxylic acid methyl ester

Guidance literature:: acryloyl chloride; With 1-butyl-5-hydroxymethyl-3-methyl-3H-imidazol-1-ium NTf₂; triethylamine; 3-butyl-5-hydroxymethyl-1-methyl-3H-imidazol-1-ium triflimide; In dichloromethane; at -20 ℃; for 0.5h;

isoprene; With hydroquinone; at 120 ℃; for 12h;

methanol; With potassium cyanide; for 12h;
DOI:10.1016/j.tetlet.2003.09.121