METHYLAMINE-N,N-D2

Base Information

• Chemical Name: METHYLAMINE-N,N-D2
• CAS No.: 2614-35-9
• Molecular Formula: CH3 D2 N
• Molecular Weight: 33.0415
• Mol file: 2614-35-9.mol

Synonyms:Methylamine-d2(6CI,7CI,8CI); Methylamine-N,N-d2

Chemical Property of METHYLAMINE-N,N-D2

Chemical Property:

• Melting Point: -93 °C(lit.)
• Boiling Point: -6.3 °C(lit.)
• Flash Point: °C
• PSA: 26.02000
• Density: 0.678g/cm³
• LogP: 0.27520

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYLAMINE-N,N-D2

There total 6 articles about METHYLAMINE-N,N-D2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylamine (74-89-5) → N-deuteriomethylamine (2614-35-9)

Guidance literature:

With nickel; deuterium; at 185 - 190 ℃;

Reference yield:

methylamine hydrochloride (593-51-1) → N-deuteriomethylamine (2614-35-9)

Guidance literature:

With water-d2; calcium oxide;

DOI:10.1039/jr9370000127

Reference yield:

methylamine (74-89-5) → N-deuteriomethylamine (2614-35-9) + monomethylamine-d2 (10477-25-5)

Guidance literature:

With deuterium hydride; methylamine; potassium salt; at -50 - 5 ℃; for 12h; Equilibrium constant; Product distribution;

DOI:10.1021/j100454a013

upstream raw materials:

methylamine hydrochloride

methylamine

N-(2-nitrovinyl)-N-methylamine

dideuterio-methyl-amine; deuteronated form

Downstream raw materials:

hydrogen cyanide

deuterio-methyl-aminyl

deuterio-methylene-amine