Silane, (1,1-dimethylethyl)diphenyl[[(2R,3R)-tetrahydro-5-methoxy-2-[2-(phenyl methoxy)ethyl]-3-furanyl]methoxy]-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)diphenyl[[(2R,3R)-tetrahydro-5-methoxy-2-[2-(phenyl methoxy)ethyl]-3-furanyl]methoxy]-
CAS No.:651020-31-4
Molecular Formula:C31H40O4Si
Molecular Weight:504.742
Hs Code.:

Synonyms:

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Chemical Property of Silane, (1,1-dimethylethyl)diphenyl[[(2R,3R)-tetrahydro-5-methoxy-2-[2-(phenyl methoxy)ethyl]-3-furanyl]methoxy]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, (1,1-dimethylethyl)diphenyl[[(2R,3R)-tetrahydro-5-methoxy-2-[2-(phenyl methoxy)ethyl]-3-furanyl]methoxy]-

There total 8 articles about Silane, (1,1-dimethylethyl)diphenyl[[(2R,3R)-tetrahydro-5-methoxy-2-[2-(phenyl methoxy)ethyl]-3-furanyl]methoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22273-77-4
((but-3-yn-1-yloxy)methyl)benzene

: 651020-31-4
methyl 6-O-benzyl-3-[[[(tert-butyl)diphenylsilyl]oxy]methyl]-2,3,5-trideoxy-D-erythro-hexofuranoside

Guidance literature:: Multi-step reaction with 7 steps

1.1: MeLi / tetrahydrofuran; diethyl ether / 0.5 h / -78 - -20 °C

1.2: 93 percent / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: 96 percent / H₂; quinoline / Lindlar catalyst / ethyl acetate

3.1: tetraisopropyl orthotitanate; (+)-diisopropyl L-tartrate; t-BuOOH / CH₂Cl₂ / -50 - -20 °C

3.2: 4.0 g / diethyl ether; tetrahydrofuran / 1 h / -50 °C

4.1: 87 percent / pyridine / CH₂Cl₂ / 20 °C

5.1: osmium tetroxide; 4-methylmorpholine 4-oxide / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 20 °C

6.1: sodium metaperiodate / tetrahydrofuran; H₂O / 0.5 h

7.1: 6.2 g / Dowex 50*8 / 1.5 h / 20 °C

With pyridine; quinoline; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; osmium(VIII) oxide; L-(+)-diisopropyl tartrate; Dowex 50*8; methyllithium; hydrogen; 4-methylmorpholine N-oxide; Lindlar's catalyst; In tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1002/hlca.200390243

Reference yield:

: 22273-79-6
5-benzyloxy-2-pentyn-1-ol

: 651020-31-4
methyl 6-O-benzyl-3-[[[(tert-butyl)diphenylsilyl]oxy]methyl]-2,3,5-trideoxy-D-erythro-hexofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: 96 percent / H₂; quinoline / Lindlar catalyst / ethyl acetate

2.1: tetraisopropyl orthotitanate; (+)-diisopropyl L-tartrate; t-BuOOH / CH₂Cl₂ / -50 - -20 °C

2.2: 4.0 g / diethyl ether; tetrahydrofuran / 1 h / -50 °C

3.1: 87 percent / pyridine / CH₂Cl₂ / 20 °C

4.1: osmium tetroxide; 4-methylmorpholine 4-oxide / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 20 °C

5.1: sodium metaperiodate / tetrahydrofuran; H₂O / 0.5 h

6.1: 6.2 g / Dowex 50*8 / 1.5 h / 20 °C

With pyridine; quinoline; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; osmium(VIII) oxide; L-(+)-diisopropyl tartrate; Dowex 50*8; hydrogen; 4-methylmorpholine N-oxide; Lindlar's catalyst; In tetrahydrofuran; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1002/hlca.200390243

Reference yield:

: 100-39-0
benzyl bromide

: 651020-31-4
methyl 6-O-benzyl-3-[[[(tert-butyl)diphenylsilyl]oxy]methyl]-2,3,5-trideoxy-D-erythro-hexofuranoside

Guidance literature:: Multi-step reaction with 8 steps

1.1: NaH; Bu₄NI / tetrahydrofuran / 1 h / 20 °C

1.2: 98 percent / tetrahydrofuran / 8 h / 20 °C

2.1: MeLi / tetrahydrofuran; diethyl ether / 0.5 h / -78 - -20 °C

2.2: 93 percent / tetrahydrofuran; diethyl ether / 2 h / 20 °C

3.1: 96 percent / H₂; quinoline / Lindlar catalyst / ethyl acetate

4.1: tetraisopropyl orthotitanate; (+)-diisopropyl L-tartrate; t-BuOOH / CH₂Cl₂ / -50 - -20 °C

4.2: 4.0 g / diethyl ether; tetrahydrofuran / 1 h / -50 °C

5.1: 87 percent / pyridine / CH₂Cl₂ / 20 °C

6.1: osmium tetroxide; 4-methylmorpholine 4-oxide / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 20 °C

7.1: sodium metaperiodate / tetrahydrofuran; H₂O / 0.5 h

8.1: 6.2 g / Dowex 50*8 / 1.5 h / 20 °C

With pyridine; quinoline; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; osmium(VIII) oxide; L-(+)-diisopropyl tartrate; Dowex 50*8; methyllithium; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; Lindlar's catalyst; In tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1002/hlca.200390243