Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl-

Base Information

Chemical Name:Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl-
CAS No.:651027-05-3
Molecular Formula:C12H16Br2F2Si
Molecular Weight:386.149
Hs Code.:
DSSTox Substance ID:DTXSID10459661
Nikkaji Number:J2.011.016C
Wikidata:Q82283486

Synonyms:Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl-;651027-05-3;DTXSID10459661;(3,4-Dibromo-2,6-difluorophenyl)triethylsilane

Suppliers and Price of Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:385.93356
Heavy Atom Count:17
Complexity:240

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC[Si](CC)(CC)C1=C(C(=C(C=C1F)Br)Br)F

Technology Process of Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl-

There total 4 articles about Silane, (3,4-dibromo-2,6-difluorophenyl)triethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 651027-04-2
(3,5-dibromo-2,6-difluorophenyl)triethylsilane

: 651027-05-3
(3,4-dibromo-2,6-difluorophenyl)triethylsilane

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -75 ℃; for 2h;
DOI:10.1002/ejoc.200300354

Reference yield:

: 994-30-9
triethylsilyl chloride

: 651027-05-3
(3,4-dibromo-2,6-difluorophenyl)triethylsilane

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / butyllithium / hexane; tetrahydrofuran / -75 °C

2: 92 percent / sec-butyllithium; bromine / cyclohexane; tetrahydrofuran / 0.75 h

3: 82 percent / diisopropylamine; butyllithium / hexane; tetrahydrofuran / -75 °C

4: diisopropylamine; butyllithium / hexane; tetrahydrofuran / 2 h / -75 °C

With n-butyllithium; bromine; sec.-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; cyclohexane;
DOI:10.1002/ejoc.200300354

Reference yield:

: 372-18-9
1,3-Difluorobenzene

: 651027-05-3
(3,4-dibromo-2,6-difluorophenyl)triethylsilane

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / butyllithium / hexane; tetrahydrofuran / -75 °C

2: 92 percent / sec-butyllithium; bromine / cyclohexane; tetrahydrofuran / 0.75 h

3: 82 percent / diisopropylamine; butyllithium / hexane; tetrahydrofuran / -75 °C

4: diisopropylamine; butyllithium / hexane; tetrahydrofuran / 2 h / -75 °C

With n-butyllithium; bromine; sec.-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; cyclohexane;
DOI:10.1002/ejoc.200300354