3-Chloro-6-hydrazinyl-4-methylpyridazine

Base Information

• Chemical Name: 3-Chloro-6-hydrazinyl-4-methylpyridazine
• CAS No.: 66530-56-1
• Molecular Formula: C5H7ClN4
• Molecular Weight: 158.59
• DSSTox Substance ID: DTXSID80495152
• Wikidata: Q82343109

Synonyms:3-Chloro-6-hydrazinyl-4-methylpyridazine;66530-56-1;(6-chloro-5-methylpyridazin-3-yl)hydrazine;SCHEMBL1189327;DTXSID80495152;YFRCRDSKRAPAOL-UHFFFAOYSA-N;AKOS006334057;3-chloro-4-methyl-6-hydrazinopyridazine;CS-0365988;A914226;3-Chloro-6-hydrazono-4-methyl-1,6-dihydropyridazine

Chemical Property of 3-Chloro-6-hydrazinyl-4-methylpyridazine

Chemical Property:

• Melting Point: 158 °C(Solv: water (7732-18-5); ethanol (64-17-5))
• Boiling Point: 275.5±23.0 °C(Predicted)
• PKA: 5.48±0.20(Predicted)
• Density: 1.52±0.1 g/cm3(Predicted)
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
• XLogP3: 0.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 158.0359239
• Heavy Atom Count: 10
• Complexity: 110

Purity/Quality:

97% ^*data from raw suppliers

3-Chloro-6-hydrazinyl-4-methylpyridazine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=NN=C1Cl)NN

Technology Process of 3-Chloro-6-hydrazinyl-4-methylpyridazine

There total 3 articles about 3-Chloro-6-hydrazinyl-4-methylpyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

3,6-dichloro-4-methylpyridazine (19064-64-3) → (6-chloro-5-methylpyridazin-3-yl)hydrazine (66530-56-1) + 6-chloro-3-hydrazino-4-methylpyridazine (66530-55-0)

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 24h;

DOI:10.1135/cccc20051372

Reference yield: 63.0%

3,6-dichloro-4-methylpyridazine (19064-64-3) + acetone (67-64-1) → 3-chloro-6-(isopropylidenehydrazino)-5-methylpyridazine + (6-chloro-5-methylpyridazin-3-yl)hydrazine (66530-56-1)

Guidance literature:

3,6-dichloro-4-methylpyridazine; With hydrazine hydrate; In ethanol; at 20 ℃; for 24h;

acetone; In hexane; column chromatography;

DOI:10.1135/cccc20051372

Reference yield:

→ (6-chloro-5-methylpyridazin-3-yl)hydrazine (66530-56-1)

Guidance literature:

3,6-Dichlor-4-methylpyridazin, N2H4*H2O (50percentig, Sdet.), neben 3-Chlor-6-hydrazino-5-methyl-pyridazin (II);

upstream raw materials:

3,6-dichloro-4-methylpyridazine

acetone

Downstream raw materials:

6-chloro-7-methyl[1,2,4]triazolo[4,3-b]pyridazine

6-chloro-3,7-dimethyl[1,2,4]triazolo[4,3-b]pyridazine

6-chloro-5-methylpyridazin-3-amine

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