2-hydroxy-N,N-dimethyl-3-nitrobenzamide

Base Information

Chemical Name:2-hydroxy-N,N-dimethyl-3-nitrobenzamide
CAS No.:66952-65-6
Molecular Formula:C9H10N2O4
Molecular Weight:210.189
Hs Code.:
DSSTox Substance ID:DTXSID30463720
Wikidata:Q82288734

Synonyms:2-hydroxy-N,N-dimethyl-3-nitrobenzamide;66952-65-6;2-hydroxy-N,N-dimethyl-3-nitro-benzamide;SCHEMBL1706905;DTXSID30463720;RVYOMZYDBIGQJO-UHFFFAOYSA-N;CS-M1414;AKOS030577283;CS-13901;FT-0758902

Suppliers and Price of 2-hydroxy-N,N-dimethyl-3-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemScene
2-Hydroxy-N,N-dimethyl-3-nitrobenzamide
1g
$ 275.00

Total 6 raw suppliers

Chemical Property of 2-hydroxy-N,N-dimethyl-3-nitrobenzamide

Chemical Property:

Melting Point:108-109 °C(Solv: ethanol (64-17-5))
Boiling Point:353.6±32.0 °C(Predicted)
PKA:5.55±0.10(Predicted)
PSA：86.36000
Density:1.356±0.06 g/cm3(Predicted)
LogP:1.52540
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:210.06405680
Heavy Atom Count:15
Complexity:261

Purity/Quality:

≥95% ^*data from raw suppliers

2-Hydroxy-N,N-dimethyl-3-nitrobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C(=O)C1=C(C(=CC=C1)[N+](=O)[O-])O

Technology Process of 2-hydroxy-N,N-dimethyl-3-nitrobenzamide

There total 6 articles about 2-hydroxy-N,N-dimethyl-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 85-38-1
3-nitrosalicylic acid

: 124-40-3
dimethyl amine

: 66952-65-6
2-hydroxy-N,N-dimethyl-3-nitrobenzamide

Guidance literature:: 3-nitrosalicylic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 24h;

dimethyl amine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield: 61.1%

: 85-38-1
3-nitrosalicylic acid

: 109-89-7
diethylamine

: 66952-65-6
2-hydroxy-N,N-dimethyl-3-nitrobenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; at 20 ℃; for 16h;