(2,5-Dichloro-4-trimethylsilyloxyphenoxy)trimethylsilane

Base Information

• Chemical Name: (2,5-Dichloro-4-trimethylsilyloxyphenoxy)trimethylsilane
• CAS No.: 67289-04-7
• Molecular Formula: C12H20Cl2O2Si2
• Molecular Weight: 323.367
• DSSTox Substance ID: DTXSID40497915
• Wikidata: Q82347686

Synonyms:67289-04-7;(2,5-Dichloro-4-trimethylsilyloxyphenoxy)trimethylsilane;DTXSID40497915;MIWBIZCTZOKMJI-UHFFFAOYSA-N;2,5-Dichlorohydroquinone, 2TMS derivative;1,4-Benzenediol, 2,5-dichloro, bis-TMS;2,5-Dichlorobenzene-1,4-diol bis-TMS ether;[(2,5-Dichloro-1,4-phenylene)bis(oxy)]bis(trimethylsilane)

Chemical Property of (2,5-Dichloro-4-trimethylsilyloxyphenoxy)trimethylsilane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 322.0378883
• Heavy Atom Count: 18
• Complexity: 248

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)OC1=CC(=C(C=C1Cl)O[Si](C)(C)C)Cl

Technology Process of (2,5-Dichloro-4-trimethylsilyloxyphenoxy)trimethylsilane

There total 3 articles about (2,5-Dichloro-4-trimethylsilyloxyphenoxy)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,2,2,2-hexamethyldisilane (1450-14-2) + 2,5-Dichloro-1,4-benzoquinone (615-93-0) → chloro-trimethyl-silane (75-77-4) + 1,4-Dichloro-2,5-bis-trimethylsilanyloxy-benzene (67289-04-7) + 2,5-Dichloro-4-trimethylsilanyloxy-phenol (139398-12-2)

Guidance literature:

In chloroform; for 0.166667h; Irradiation;

DOI:10.1016/0022-328X(91)86427-R

Reference yield:

1,1,1,2,2,2-hexamethyldisilane (1450-14-2) + 2,5-Dichloro-1,4-benzoquinone (615-93-0) → 1,4-Dichloro-2,5-bis-trimethylsilanyloxy-benzene (67289-04-7)

Guidance literature:

With iodine; In benzene; at 80 ℃; for 7h;

DOI:10.1246/cl.1982.533

Reference yield:

→ 1,4-Dichloro-2,5-bis-trimethylsilanyloxy-benzene (67289-04-7)

Guidance literature:

2-Chlorbenzochinon 1. (CH3)3SiCl 2. (CH3)4NCl, in CH3CN 3. <(CH3)3Si>2NH;

DOI:10.1021/jo00409a039

upstream raw materials:

1,1,1,2,2,2-hexamethyldisilane

2,5-Dichloro-1,4-benzoquinone

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