Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester

Base Information

Chemical Name:Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester
CAS No.:68621-77-2
Molecular Formula:C9H12N2O2
Molecular Weight:180.206
Hs Code.:
DSSTox Substance ID:DTXSID80450822
Nikkaji Number:J31.243F
Wikidata:Q82270643

Synonyms:68621-77-2;Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester;SCHEMBL10782684;DTXSID80450822;AKOS000204034;2-Methyl-5-(methoxycarbonylamino)aniline

Suppliers and Price of Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:180.089877630
Heavy Atom Count:13
Complexity:185

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)NC(=O)OC)N

Technology Process of Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester

There total 15 articles about Carbamic acid, (3-amino-4-methylphenyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 95-80-7,71111-07-4
4-methylbenzene-1,3-diamine

: 616-38-6
carbonic acid dimethyl ester

: 68621-77-2
methyl (3-amino-4-methylphenyl)carbamate

: 6935-99-5
2,4-bis(methoxycarbonylamino)toluene

: N-(5-amino-2-methylphenyl)carbamic acid methyl ester

Guidance literature:: Fe/CeO₂; for 8h; Product distribution / selectivity; vial which can withstand pressure;

Reference yield: 63.0%

: 121-14-2
2,4-dinitrotoluene

: 616-38-6
carbonic acid dimethyl ester

: 68621-77-2
methyl (3-amino-4-methylphenyl)carbamate

: 6935-99-5
2,4-bis(methoxycarbonylamino)toluene

: N-(5-amino-2-methylphenyl)carbamic acid methyl ester

Guidance literature:: With hydrogen; 1 wt% Au/CeO₂; at 150 ℃; for 23h; under 11251.1 Torr; Product distribution / selectivity; Inert atmosphere;

Reference yield: 62.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 121-14-2
2,4-dinitrotoluene

: 68621-77-2
methyl (3-amino-4-methylphenyl)carbamate

: 6935-99-5
2,4-bis(methoxycarbonylamino)toluene

Guidance literature:: With [2,2]bipyridinyl; dodecacarbonyl-triangulo-triruthenium; montmorillonitebipyridynylpalladium(II) acetate (Pd-clay); In benzene; at 180 ℃; for 24h; under 53200 Torr;
DOI:10.1021/ja00062a055