Selenazole, 2,4-diphenyl-

Base Information

• Chemical Name: Selenazole, 2,4-diphenyl-
• CAS No.: 69625-83-8
• Molecular Formula: C15H11NSe
• Molecular Weight: 284.219
• Mol file: 69625-83-8.mol

Synonyms:

Chemical Property of Selenazole, 2,4-diphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Selenazole, 2,4-diphenyl-

There total 4 articles about Selenazole, 2,4-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

morpholino(phenyl)-methaneselenone (31646-06-7) + 1-(1-azido-2-iodoethyl)benzene (4098-17-3) → 2,4-diphenyl-1,3-selenazole (69625-83-8)

Guidance literature:

With potassium tert-butylate; at 80 ℃; for 7h;

DOI:10.1021/acscombsci.9b00045

Reference yield: 87.0%

α-bromoacetophenone (70-11-1) + selenobenzamide (5977-82-2) → 2,4-diphenyl-1,3-selenazole (69625-83-8)

Guidance literature:

In ethanol; Heating;

DOI:10.1055/s-2002-35604

Reference yield: 78.0%

acetophenone (98-86-2) + selenobenzamide (5977-82-2) → 2,4-diphenyl-1,3-selenazole (69625-83-8)

Guidance literature:

acetophenone; With [hydroxy(tosyloxy)iodo]benzene; In acetonitrile; for 0.5h; Heating;

selenobenzamide; In methanol; for 0.5h; Heating;

DOI:10.1055/s-2000-6407

upstream raw materials:

α-bromoacetophenone

selenobenzamide

acetophenone

morpholino(phenyl)-methaneselenone

Downstream raw materials:

3,4-bis(methoxycarbonyl)-2,6-diphenylpyridine