Butyl 2-methoxyethyl ether

Base Information

• Chemical Name: Butyl 2-methoxyethyl ether
• CAS No.: 13343-98-1
• Molecular Formula: C7H16 O2
• Molecular Weight: 132.203
• Hs Code.: 2909199090
• European Community (EC) Number: 236-392-7
• DSSTox Substance ID: DTXSID00928119
• Nikkaji Number: J100.454I
• Wikidata: Q82902852
• Mol file: 13343-98-1.mol

Synonyms:Butyl 2-methoxyethyl ether;13343-98-1;2,5-Dioxanonane;1-(2-Methoxyethoxy)butane;Butane, 1-(2-methoxyethoxy)-;1-Butoxy-2-methoxyethane;Ethane, 1-butoxy-2-methoxy-;EINECS 236-392-7;500005-29-8;Butyl2-methoxyethylether;1-(2-Methoxyethoxy) butane;SCHEMBL531049;DTXSID00928119;MFCD01366355;AKOS028108523;AS-58663;CS-0196688

Chemical Property of Butyl 2-methoxyethyl ether

Chemical Property:

• Vapor Pressure: 5.71mmHg at 25°C
• Melting Point: -15.45°C (estimate)
• Refractive Index: 1.4196 (estimate)
• Boiling Point: 147°Cat760mmHg
• Flash Point: 25.2°C
• PSA: 18.46000
• Density: 0.843g/cm³
• LogP: 1.44950
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 132.115029749
• Heavy Atom Count: 9
• Complexity: 46.2

Purity/Quality:

98%Min ^*data from raw suppliers

BUtyl2-methoxyethylether 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCOCCOC

Technology Process of Butyl 2-methoxyethyl ether

There total 13 articles about Butyl 2-methoxyethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

trimethyl phosphite (512-56-1) + 2-Butoxyethanol (111-76-2,9004-77-7) → 1-(2-methoxy-ethoxy)-butane (13343-98-1)

Guidance literature:

With PPA; at 180 - 190 ℃; for 2h;

DOI:10.3891/acta.chem.scand.52-1223

Reference yield:

1,1-bis-(2-methoxy-ethoxy)-butane (71808-63-4) → 2-Butoxyethanol (111-76-2,9004-77-7) + 1-(2-methoxy-ethoxy)-butane (13343-98-1)

Guidance literature:

With nickel; at 200 - 240 ℃; under 51485.6 - 77228.3 Torr; Hydrogenation;

Reference yield:

oxirane (75-21-8,99932-75-9) + methanol (67-56-1) + 1-butyl-1-nitrosourea (869-01-2) → butyl methyl ether (628-28-4) + 2-butyl methyl ether (6795-87-5) + 1-(2-methoxy-ethoxy)-butane (13343-98-1) + 1-<2-(2-Methoxyethoxy)ethoxy>butan (7382-32-3)

Guidance literature:

With sodium hydrogencarbonate; Further byproducts given; Ambient temperature;

upstream raw materials:

1,1-bis-(2-methoxy-ethoxy)-butane

oxirane

methanol

1-butyl-1-nitrosourea

Refernces

• 1、 Kirmse, Wolfgang,Jansen, Ulrich. "Deamination Reactions, 41. Reactions of Aliphatic Diazonium Ions and Carbocations with Ethers". . p. 2607 - 2625. Retrieved 2007/10/02.