tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane

Base Information

Chemical Name:tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane
CAS No.:72726-56-8
Molecular Formula:C13H26OSi
Molecular Weight:226.434
Hs Code.:
DSSTox Substance ID:DTXSID10502863
Nikkaji Number:J1.734.429C

Synonyms:72726-56-8;SCHEMBL9285252;tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane;DTXSID10502863

Suppliers and Price of tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:226.175291983
Heavy Atom Count:15
Complexity:237

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OC1CCCCC1=C

Technology Process of tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane

There total 8 articles about tert-Butyl(dimethyl)[(2-methylidenecyclohexyl)oxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 127375-62-6
(Bicyclo[4.1.0]hept-1-yloxy)-tert-butyl-dimethyl-silane

: 72726-56-8
tert-butyl(dimethyl)[(2-methylenecyclohexyl)oxy]silane

Guidance literature:: With Zeise's dimer; In chloroform; at 20 ℃;
DOI:10.1021/ja00030a080

Reference yield: 71.0%

: 74173-08-3
2-(tert-Butyldimethylsilyloxy)-1-cyclohexanon

: 18107-18-1
diazomethyl-trimethyl-silane

: 72726-56-8
tert-butyl(dimethyl)[(2-methylenecyclohexyl)oxy]silane

Guidance literature:: With triphenylphosphine; isopropyl alcohol; Wilkinson's catalyst; In 1,4-dioxane; at 60 ℃; for 4h;
DOI:10.1021/ol049085p

Reference yield: 52.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 74173-08-3
2-(tert-Butyldimethylsilyloxy)-1-cyclohexanon

: 72726-56-8
tert-butyl(dimethyl)[(2-methylenecyclohexyl)oxy]silane

Guidance literature:: Methyltriphenylphosphonium bromide; With sodium hexamethyldisilazane; In 1,4-dioxane; at 60 ℃; for 1h;

2-(tert-Butyldimethylsilyloxy)-1-cyclohexanon; In 1,4-dioxane; at 60 ℃; for 4h;
DOI:10.1021/ol049085p