Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)-

Base Information

Chemical Name:Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)-
CAS No.:75390-40-8
Molecular Formula:C30H30N4
Molecular Weight:446.595
Hs Code.:
DSSTox Substance ID:DTXSID50412952
Nikkaji Number:J1.333.040I

Synonyms:75390-40-8;Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)-;DTXSID50412952

Suppliers and Price of Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)-

Chemical Property:

XLogP3:7.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:446.24704697
Heavy Atom Count:34
Complexity:595

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NC(=NC2=CC=C(C=C2)C)C(=NC3=CC=C(C=C3)C)NC4=CC=C(C=C4)C

Technology Process of Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)-

There total 2 articles about Ethanediimidamide, N,N',N'',N'''-tetrakis(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106-49-0,12221-03-3
p-toluidine

: 7472-70-0
N,N'-di(p-tolyl)oxaldiimidoyl dichloride

: 75390-40-8
tetra-p-tolyloxalic amidine

Guidance literature:: In benzene; for 2h; Heating;

Reference yield:

: 75390-40-8
N⁽¹⁾,N⁽²⁾,N⁽³⁾,N⁽⁴⁾-tetra(p-tolyl)oxalamidine

Guidance literature:: Oxalimidoylchlorid, entspr. Amin;

Reference yield: 94.0%

: 15709-76-9
tris(triphenylphosphino)copper(I) chloride

: 60-29-7,927820-24-4
diethyl ether

: 75390-40-8
N⁽¹⁾,N⁽²⁾,N⁽³⁾,N⁽⁴⁾-tetra(p-tolyl)oxalamidine

: tetra(p-tolyl)-oxalamidinato-bis[bis(triphenylphosphine)-copper(I)]*1.5 diethyl ether

Guidance literature:: With MeLi; In tetrahydrofuran; diethyl ether; byproducts: LiCl, PPh3; soln. of oxalic amidine in THF reacted with 2 equiv. of soln. of MeLi inEt2O at -78°C, warmed to room temp. by stirring, soln. of Cu com pd. added dropwise, stirred at room temp. for 12 h; solvent evapd. in cold, crystd. at -25°C for 12 h, filtered, washed with Et2O, dried in vac., recrystd. from CH2Cl2/Et2O, elem. anal.;
DOI:10.1002/zaac.200300034