1,3-Propanediol, 2-methoxy-

Base Information

• Chemical Name: 1,3-Propanediol, 2-methoxy-
• CAS No.: 761-06-8
• Molecular Formula: C4H10O3
• Molecular Weight: 106.122
• European Community (EC) Number: 822-386-7
• UNII: 3GSZ82L6KV
• DSSTox Substance ID: DTXSID70457486
• Nikkaji Number: J323.891A
• Wikidata: Q27257189
• RXCUI: 2604173

Synonyms:2-methoxypropane-1,3-diol;761-06-8;1,3-Propanediol, 2-methoxy-;2-methoxy-1,3-propanediol;Glycerin 2-methyl ether;2-O-Methylglycerol;Glycerol 2-methyl ether;2-methylglycerin;2-methylglycerol;3GSZ82L6KV;2-O-methylglycerin;2-O-methyl-glycerol;2-methoxy-propane-1,3-diol;1,3-Propanediol, 2-methoxy;SCHEMBL360480;2-methoxy-1,3-propyleneglycol;DTXSID70457486;MFCD00672589;AKOS006271970;SY316320;EN300-128506;Q27257189

Chemical Property of 1,3-Propanediol, 2-methoxy-

Chemical Property:

• Vapor Pressure: 0.0113mmHg at 25°C
• XLogP3: -1.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 106.062994177
• Heavy Atom Count: 7
• Complexity: 33.9

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(CO)CO

Technology Process of 1,3-Propanediol, 2-methoxy-

There total 10 articles about 1,3-Propanediol, 2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) + dimethyl sulfate (77-78-1) → glycerol 1-monomethyl ether (623-39-2,36887-04-4) + 2-methylglycerol (761-06-8)

Guidance literature:

With sodium hydroxide; at 90 - 100 ℃;

DOI:10.1023/A:1022224828164

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 5-methoxy-2-phenyl-1,3-dioxane (104216-84-4) → 2-methylglycerol (761-06-8) + benzaldehyde (100-52-7)

Guidance literature:

Reference yield:

5-methoxy-1,3-dioxane (99586-36-4) + hydrogenchloride (7647-01-0,15364-23-5) → formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-methylglycerol (761-06-8)

Guidance literature:

upstream raw materials:

glycerol

5-methoxy-1,3-dioxane

hydrogenchloride

5-methoxy-2-(4-nitro-phenyl)-[1,3]dioxane

Downstream raw materials:

5-methoxytrimethylenephosphoric acid phenyl ester

rac.-1-Stearoyl-glycerin-methylaether-2

2-O-Methyl-1,3-di-O-p-phenylazobenzoyl-glycerin

3-(hexadecyloxy)-2-methoxy-1-propanol

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