Ethyl 5,6-Dimethylnicotinate

Base Information

Chemical Name:Ethyl 5,6-Dimethylnicotinate
CAS No.:77629-53-9
Molecular Formula:C10H13NO2
Molecular Weight:179.21600
Hs Code.:
Mol file:77629-53-9.mol

Synonyms:Ethyl 5,6-Dimethylnicotinate;ethyl 5,6-dimethyl-3-pyridinecarboxylate;3-Pyridinecarboxylic acid,5,6-dimethyl-,ethyl ester;

Suppliers and Price of Ethyl 5,6-Dimethylnicotinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ethyl5,6-Dimethylnicotinate
2g
$ 920.00

AOBChem
Ethyl5,6-dimethylpyridine-3-carboxylate 95%
25g
$ 3457.00

Total 3 raw suppliers

Chemical Property of Ethyl 5,6-Dimethylnicotinate

Chemical Property:

Vapor Pressure:0.0105mmHg at 25°C
Boiling Point:263.1oC at 760 mmHg
Flash Point:112.9oC
PSA：39.19000
Density:1.056g/cm3
LogP:1.87510
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

Ethyl5,6-Dimethylnicotinate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Ethyl 5,6-Dimethylnicotinate can be eluated from filling material used in dentistry, as well as an intermediate in the preparation of Omeprazole metabolites. Eluate from filling material used in dentistry, as well as an intermediate in the preparation of Omeprazole metabolites.

Technology Process of Ethyl 5,6-Dimethylnicotinate

There total 4 articles about Ethyl 5,6-Dimethylnicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 64-17-5
ethanol

: 113124-10-0
5-carboxy-2,3-dimethylpyridinium chloride

: 77629-53-9
ethyl 5,6-dimethyl-3-pyridinecarboxylate

Guidance literature:: With orthoformic acid triethyl ester; for 4.5h; Heating;

Reference yield: 75.0%

: 77629-52-8
Ethyl 2,4-Dichloro-5,6-dimethylnicotinate

: 77629-53-9
ethyl 5,6-dimethyl-3-pyridinecarboxylate

Guidance literature:: With hydrogen; sodium acetate; palladium dichloride; In ethanol; for 22h; under 2585.7 Torr;
DOI:10.1021/jo00328a010

Reference yield:

: 77629-51-7
Ethyl 2,4-Dihydroxy-5,6-dimethylnicotinate

: 77629-53-9
ethyl 5,6-dimethyl-3-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / phosphorus oxychloride / 6 h / 120 °C / Parr bomb

2: 75 percent / H₂, palladium chloride, CH₃COONa / ethanol / 22 h / 2585.7 Torr

With hydrogen; sodium acetate; palladium dichloride; trichlorophosphate; In ethanol;
DOI:10.1021/jo00328a010